Preparation and optical properties of nickel nanoparticles implanted carbon membranes

Disha Harinkhere, K. Choudhary, N. Kaurav
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引用次数: 1

Abstract

Through dip coating method monodisperse nickel nanoparticles assisted carbon membrane was prepared on porous alumina disc support. The coating solution was prepared by blending of thermally stable polymer polyphenylene oxide (PPO) and thermally labile polymer polyvinylpyrrolidone (PVP) followed by addition of nickel nanoparticles. Size of nanoparticles, surface porosity, average pore size, element composition and optical properties of the membrane were investigated by means of different techniques such as XRD, FE-SEM, EDS and UV-Visible spectrometer Incorporation of nano-sized nickel in polymer matrix causes increase in pore size from 0.022 μm to 0.076 μm as well as porosity and decrease in optical band gap from 5.44 eV to 5.09 eV of membrane.
纳米镍植入碳膜的制备及其光学性能
采用浸涂法在多孔氧化铝圆盘载体上制备了单分散镍纳米颗粒辅助碳膜。采用热稳定型聚合物聚苯乙烯氧化物(PPO)和热不稳定型聚合物聚乙烯吡咯烷酮(PVP)共混,并加入纳米镍制备涂层溶液。采用XRD、FE-SEM、EDS、uv -可见光谱等不同技术研究了纳米颗粒的尺寸、表面孔隙率、平均孔径、元素组成和膜的光学性能,纳米镍在聚合物基体中的掺入使膜的孔径从0.022 μm增大到0.076 μm,孔隙率从5.44 eV减小到5.09 eV,光学带隙从5.44 eV减小。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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