The Influence of Nanosized Zirconium (IV) Oxide on the Catalytic Curing of Epoxy Resin ED-20 with Isomethyltetrahydrophthalic Anhydride

E. Shved, Yuliia Bespalko, O. Gorban, K. Yutilova, E. Bakhalova
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Abstract

The effect of the filler – the nanoparticles of zirconium (IV) oxide (16.5nm) on the thermal stability of composites based on epoxy resin ED-20, isomethyltetrahydrophthalic anhydride, complex catalyst, and plasticizer has been studied. The yield of the sol fraction of composites with different content of ZrO2 nanoparticles has been evaluated by the derivatography method. The resistance of the obtained polymers and composites to thermal oxidative degradation has been evaluated by derivatography. Evaluation of the effectiveness of the influence of ZrO2 on the curing has been carried out according to the data of differential scanning calorimetry (DSC) by the Kissinger method. The optimal content of ZrO2 in the composition has been established.
纳米氧化锆对异甲基四氢邻苯二酸酐催化固化环氧树脂ED-20的影响
研究了填料——氧化锆纳米颗粒(16.5nm)对环氧树脂ED-20、异甲基四氢苯酐、络合催化剂和增塑剂复合材料热稳定性的影响。采用衍生法对不同ZrO2纳米颗粒含量的复合材料溶胶组分的收率进行了评价。所得的聚合物和复合材料的抗热氧化降解性能通过衍生法进行了评价。根据差示扫描量热法(DSC)的数据,用Kissinger法评价了ZrO2对固化影响的有效性。确定了ZrO2在合成物中的最佳含量。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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