Santosh S. Katkar, A. H. Kategaonkar, Kaluram N. Vidhate
{"title":"MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones","authors":"Santosh S. Katkar, A. H. Kategaonkar, Kaluram N. Vidhate","doi":"10.23939/chcht14.02.169","DOIUrl":null,"url":null,"abstract":"We have studied a series of mixed metal oxides of Mg-Al by a simple co-precipitation technique. Various characterization techniques, including XRD, SEM, EDS, TEM, BET and CO2-TPD were carried out to investigate their physicochemical properties. An efficient and facile protocol has been documented for the synthesis of chalcones using different aldehydes and acetophenone using Mg-Al oxide under reflux conditions in ethanol affording good to excellent yields. Recyclability of a catalyst is a significant feature of this protocol. Moreover, it was proposed that MgO can disperse and increase the basicity, pore size and catalytic activity.","PeriodicalId":9762,"journal":{"name":"Chemistry and Chemical Technology","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2020-06-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemistry and Chemical Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.23939/chcht14.02.169","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
Abstract
We have studied a series of mixed metal oxides of Mg-Al by a simple co-precipitation technique. Various characterization techniques, including XRD, SEM, EDS, TEM, BET and CO2-TPD were carried out to investigate their physicochemical properties. An efficient and facile protocol has been documented for the synthesis of chalcones using different aldehydes and acetophenone using Mg-Al oxide under reflux conditions in ethanol affording good to excellent yields. Recyclability of a catalyst is a significant feature of this protocol. Moreover, it was proposed that MgO can disperse and increase the basicity, pore size and catalytic activity.