Factorial Design Validation of an Environmentally Benign Water-Based Drilling Fluid from Sweet Potato Peels at Elevated Temperatures

Ifeanyichukwu Ebuzeme, O. Olatunji, B. Olufemi
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引用次数: 1

Abstract

In recent years, several research types have been carried out to produce environmentally-benign drilling fluid additives using locally sourced substances. Still, the formulation of a more effective and cheaper viscosifier for a better hole cleaning ability that lowers risk in lost circulation zones, especially at higher temperatures, remains a critical research subject. This study examines the use of Sweet Potato Peels Extract (PPE), a more readily available by-product, as a drilling fluid additive. A 23 factorial experiment that considers temperature, PPE and Xanthan Gum (X.G.) as factor variables and viscosity as a response variable was conducted for field optimisation. In this research, the PPE and other commercial polymers were measured at different concentrations and combined in a specified ratio of 1:1 by mass to verify the levels of interaction between the additives on the mud weight, yield point (Y.P.), and plastic viscosity (P.V.) of the formulated drilling mud. The additives’ effects were then recorded using a mud balance, a viscometer, and a heater for temperature variance. The results were then compared with the control mud to ascertain the additives’ effectiveness. Experimental results revealed that the PPE and X.G. increased the Y.P. and P.V. at 104 °F and 176 °F, respectively. On adding 6 g of X.G. to the control mud (8.97 ppg), at 104 °F and 176 °F, the Y.P. increased by 88% and 11%, respectively, and the 3 g PPE + 3 g X.G. gave a better inference at 104 °F and 176 °F with a 92% and 38% increase respectively. This increase is a result of higher potassium content in the PPE from chemical laboratory analysis. Apart from the optimum ratio by mass of 1:1 above, the combination effects or results are shown using the factorial design experiment. The factor variables were modelled into a mathematical equation that indicates PPE additive as the most significant parameter on the yield point. The second component of viscosity, plastic viscosity (P.V.), followed a similar trend. Furthermore, PPE and X.G.'s effect on plastic viscosity at 176 °F decreased slightly with an increase in the control mud's salinity. This novel combination offers a more cost-effective and better-performing viscosifier than the conventional X.G. from the above results. The model helps predict downhole conditions better as it shows the interactive effects of the various additives and can help inform decisions at the surface. A better hole cleaning ability, lower risk in lost circulation zones, and reduced Non-Productive Time would be the benefits of using this formulation.
高温甘薯皮制备的环保型水基钻井液的析因设计验证
近年来,已经开展了几种类型的研究,以使用本地物质生产环保型钻井液添加剂。尽管如此,寻找一种更有效、更便宜的增粘剂,以提高井眼清洁能力,降低井眼漏失风险,特别是在高温下,仍然是一个重要的研究课题。本研究考察了甘薯皮提取物(PPE)作为钻井液添加剂的使用,这是一种更容易获得的副产品。以温度、PPE和黄原胶(X.G.)为因素变量,粘度为响应变量,进行了23因子实验,进行了现场优化。在这项研究中,PPE和其他商业聚合物在不同浓度下进行了测量,并以1:1的特定质量比组合,以验证添加剂对泥浆重量、屈服点(Y.P.)和塑性粘度(P.V.)的相互作用水平。然后使用泥浆天平、粘度计和温度变化加热器记录添加剂的影响。然后将结果与对照泥浆进行比较,以确定添加剂的有效性。实验结果表明,PPE和X.G.分别在104°F和176°F时提高了Y.P.和P.V.。在104°F和176°F的温度下,在对照泥浆(8.97 ppg)中加入6 g的X.G., Y.P.分别提高了88%和11%,而在104°F和176°F的温度下,3g PPE + 3g X.G.的推断效果更好,分别提高了92%和38%。这一增加是化学实验室分析得出的PPE中钾含量较高的结果。除上述最佳质量比为1:1外,采用析因设计试验显示了组合效果或结果。这些因素变量被建模成一个数学方程,表明PPE添加剂是对屈服点最重要的参数。粘度的第二个组成部分,塑性粘度(P.V.),也遵循类似的趋势。此外,PPE和X.G.在176°F时,随着对照泥浆矿化度的增加,对塑性粘度的影响略有下降。从上述结果来看,这种新颖的组合提供了一种比传统的X.G.更具成本效益和更好性能的增粘剂。该模型可以更好地预测井下状况,因为它显示了各种添加剂的相互作用,并有助于为地面决策提供信息。使用该配方的好处是具有更好的井眼清洁能力、更低的漏失风险和更短的非生产时间。
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