Effect of addition of surfactant on LPG sensing properties of nano tin oxide based thick film sensors

A. Garje
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引用次数: 1

Abstract

Nanocrystalline tin oxide powder is synthesized using sol gel method. To observe the effect of addition of surfactant on particle size, Sodium Dodecyl Sulphate (SDS) is added during the synthesis. The particle is found to be ~ 8 nm using TEM. The synthesized nanophase tin oxide powder is used to fabricate thick film sensors using screen printing technique. The sensor performance is tested for 100 ppm of LPG. The role of surfactant is observed to be responsible for remarkable improvement in sensitivity for LPG by 5 times with low operating temperature of 110 °c. The optical and structural characterization of powder and film is done using UV-Vis, XRD, SEM; TEM. The repeatability, response and recovery time of the sensors is studied.
表面活性剂对纳米氧化锡基厚膜液化气传感器传感性能的影响
采用溶胶-凝胶法制备了纳米氧化锡粉体。为了观察表面活性剂的加入对颗粒大小的影响,在合成过程中加入十二烷基硫酸钠(SDS)。通过透射电镜分析,发现该粒子的粒径为~ 8 nm。采用丝网印刷技术将合成的纳米氧化锡粉末用于制作厚膜传感器。在100ppm的LPG中测试传感器的性能。在低工作温度为110℃时,表面活性剂的作用使LPG的灵敏度提高了5倍。采用UV-Vis、XRD、SEM对粉末和薄膜进行了光学和结构表征;TEM。研究了传感器的重复性、响应性和恢复时间。
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