Sintesis Mikroemulsi Menggunakan Surfaktan dan Minyak Atsiri Kulit Buah Lemon (Citrus limon) Sebagai Face Mist

Tania Suciati, Lutfi Suhendra, Bambang Admadi Harsojuwono
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Abstract

This study aims to determine the effect of the ratio of the mixture of surfactants and essential oil of lemon rind (Citrus limon) and determine the ratio of surfactant and essential oil of lemon rind (Citrus limon) to obtain the best microemulsion characteristics. This experiment used a completely randomized design with step 1 ratio of surfactant mixture (Tween 20: Tween 80: Span 80) which was 97: 2.75: 0.25; 97:2.5:0.5; 97:2.25:0.75; 97:2.0:1; 97:1.75; 1.25. Then, in step 2 the ratio of surfactant and lemon peel essential oil was 90:10; 87.5: 12.5; 85:15; 82.5:17.5; 80:20. Data were analyzed using analysis of variance using excel. The results showed that the ratio of the mixture of surfactants and lemon peel essential oil had an effect on the characteristics of the resulting microemulsion. The ratio of surfactant mixture 97: 2.75: 0.25 (Tween 20: Tween 80: Span 80) was the best treatment for making lemon peel essential oil microemulsion with the lowest turbidity values ??before and after centrifugation, namely 0.245±0.010% and 0.203±0.059 %. The ratio of surfactant and essential oil of lemon peel 85:15 was the best treatment with turbidity index values ??before and after centrifugation 0.298±0.037% and 0.334±0.161%, respectively. Lemon peel essential oil microemulsion has a particle size of 1272.2 nm and a potential zeta value of 0 mV. Lemon peel essential oil microemulsion 85:15 was stable for 8 weeks of storage.
本研究旨在确定表面活性剂与柠檬皮精油(Citrus limon)混合比例的影响,并确定表面活性剂与柠檬皮精油(Citrus limon)的比例,以获得最佳微乳液特性。实验采用完全随机设计,第一步表面活性剂配比(Tween 20: Tween 80: Span 80)为97:2.75:0.25;97:2.5:0.5;97:2.25:0.75;97:2.0:1;97:1.75;1.25. 然后在步骤2中,表面活性剂与柠檬皮精油的比例为90:10;87.5: 12.5;85:15;82.5:17.5;80:20。采用excel进行方差分析。结果表明,表面活性剂与柠檬皮精油的配比对所制微乳液的特性有影响。表面活性剂配比为97:2.75:0.25 (Tween 20: Tween 80: Span 80)时,可制得浊度最低的柠檬皮精油微乳液。离心前后分别为0.245±0.010%和0.203±0.059%。表面活性剂与柠檬皮精油的比例为85:15,浊度指数值为??离心前后分别为0.298±0.037%和0.334±0.161%。柠檬皮精油微乳液粒径为1272.2 nm,电位zeta值为0 mV。85:15柠檬皮精油微乳液保存8周稳定。
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