Synthesis of nickel nanoparticles by sol-gel method and their characterization

A. Shamim, Zaheer Ahmad, S. Mahmood, Umair Ali, T. Mahmood, Zamir Ahmad Nizami
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引用次数: 3

Abstract

The under consideration study focuses on synthesis and characterization of Nickel oxide (NiO) nanoparticles. Nanosized Nickel oxide powder was successfully synthesized using a simple and low cast sol-gel method. This method is environment friendly requiring no expensive chemicals and is time saving. The sol-gel method was accompanied by the formation of precipitates which were dried and calcined at 550oC to get nickel oxide nanoparticles. The synthesized nanopowder was characterized by X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and Energy Dispersive Spectroscopy (EDX).
溶胶-凝胶法制备纳米镍及其表征
研究重点是氧化镍纳米颗粒的合成和表征。采用简单、低铸型的溶胶-凝胶法制备了纳米氧化镍粉体。这种方法对环境友好,不需要昂贵的化学品,而且节省时间。溶胶-凝胶法制备沉淀,在550℃下干燥煅烧得到氧化镍纳米颗粒。采用x射线衍射(XRD)、扫描电镜(SEM)和能量色散光谱(EDX)对合成的纳米粉体进行了表征。
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