Microstructures of a Ni-9.6 at.% Ta-16.6 at.% Cr alloy after aging up to 1000 hours from 600 to 1,000°C

Yee C. Lin, C.R. Brooks
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Abstract

The effects of aging of a Ni-rich Ni-Ta-Cr alloy on the microstructure (using optical and scanning electron microscopy) and hardness are presented. In the solution-annealed condition (1280°C, 4 h) the microstructure consisted of a face-centered cubic matrix and about 10% of a Ni3Ta type phase, which contained some Cr; the hardness was about 530 DPH. No change in the microstructure nor significant change in hardness occurred upon aging at 600°C for 1,000 h. Aging from 700 to 1000°C produced a significant decrease in hardness, to about 330 DPH after 1000 h. A lamellar product formed, usually initiating at the secondary particles present in the solution-annealed condition. At longer times and higher temperatures, a coarser lamellar product formed. The results of qualitative EDS analysis of the phases are reported.

Ni-9.6 at的显微组织。% Ta-16.6 at。% Cr合金在600 ~ 1000℃时效后可达1000小时
研究了一种富Ni-Ta-Cr合金时效对显微组织(光学和扫描电镜观察)和硬度的影响。在1280℃,4 h的固溶退火条件下,显微组织由面心立方基体和约10%的Ni3Ta型相组成,其中含有一定量的Cr;硬度约为530 DPH。在600°C时效1000 h后,显微组织没有变化,硬度也没有明显变化。从700°C时效到1000°C,硬度显著下降,1000 h后硬度降至330 DPH左右。形成层状产物,通常起源于溶液退火条件下存在的二次颗粒。在较长的时间和较高的温度下,形成了较粗糙的片层状产物。报道了相的定性能谱分析结果。
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