Effect of solution cooling rate on the γ′ precipitation behaviors of a Ni-base P/M superalloy

Gaofeng Tian, Chengchang Jia, Ying Wen, Benfu Hu
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引用次数: 19

Abstract

The effect of cooling rate on the cooling γ′ precipitation behaviors was investigated in a Ni-base powder/metallurgy (P/M) superalloy (FGH4096). The empirical equations were established between the cooling rate and the average sizes of secondary and tertiary γ′ precipitates within grains and tertiary γ′ precipitates at grain boundaries, as well as the apparent width of grain boundaries. The results show that the average sizes of secondary or tertiary γ′ precipitates are inversely correlated with the cooling rate. The shape of secondary γ′ precipitates within grains changes from butterfly-like to spherical with the increase of cooling rate, but all the tertiary γ′ precipitates formed are spherical in shape. It is also found that tertiary γ′ may be precipitated in the latter part of the cooling cycle only if the cooling rate is not faster than 4.3°C/s, and the apparent width of grain boundaries decreases linearly with the increase of cooling rate.

固溶冷却速率对ni基P/M高温合金γ′析出行为的影响
研究了冷却速率对ni基粉末/冶金(P/M)高温合金(FGH4096)冷却γ′析出行为的影响。建立了冷却速率与晶内二次、三级γ′相平均尺寸、晶界三级γ′相平均尺寸及晶界表观宽度之间的经验方程。结果表明,二次或三级γ′析出相的平均尺寸与冷却速率呈负相关。随着冷却速率的增加,晶粒内次生γ′相的形状由蝴蝶状变为球形,而形成的次生γ′相均为球形。当冷却速率不大于4.3℃/s时,在冷却循环的后期才会析出第三系γ′,晶界表观宽度随冷却速率的增加而线性减小。
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