Some New Heterocyclisations Based on N-(2,2-dichloro-1-isothiocyanatoethyl)benzamide Derivatives

IF 0.4 Q4 CHEMISTRY, MULTIDISCIPLINARY
Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko
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引用次数: 0

Abstract

Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.
基于N-(2,2-二氯-1-异硫氰酸乙酯)苯酰胺衍生物的一些新的杂环化合物
摘要以现有的N-(2,2-二氯-1-(2-(4-甲基苯甲酰)-肼-1-碳硫氨基)乙基)苯酰胺为基础,合成了相应的N-(2,2-二氯-1-(5-(对苯基)-1,3,4-恶二唑-2-基)氨基)乙基)苯酰胺和5-(对苯基)-1,3,4-噻二唑-2-胺。产品以可接受的收率接收,并从反应混合物中分离出来,没有任何特别的困难。所得化合物的结构经1H、13C NMR和质谱数据证实。
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来源期刊
Acta Chemica Iasi
Acta Chemica Iasi CHEMISTRY, MULTIDISCIPLINARY-
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