Achieving Bi-Lamellar Microstructure with Both High Tensile Strength and Large Ductility in Ti-6Al-4V Alloy by Novel Thermomechanical Processing

Yan Chong, T. Bhattacharjee, J. Yi, Shiteng Zhao, N. Tsuji
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Abstract

In this study, a novel through-β-transus processing followed by intercritical annealing was designed to obtain the bi-lamellar microstructure in Ti-6Al-4V alloy with refined colony sizes, by which both tensile strength and ductility were significantly improved. The colony size obtained in the through-β-transus processing was 60 μm, much smaller than the minimum colony size of 130 μm that can be achieved in the conventional β processing. The colony refinement was attributed to the decreased size of the grain boundary α phase with increased variety of crystallographic orientations, which acted as nucleation sites for subsequent colony structures. By intercritical annealing of the lamellar microstructures in α+β two-phase region followed by water quenching, bi-lamellar microstructures composed of primary α lamellae and transformed β regions composed of fine secondary α plates were obtained, maintaining the same colony size as the lamellar precursors. The total elongation of bi-lamellar microstructure significantly improved from 3.4% to 18.6% with decreasing the colony size, while the high yield and tensile strength was independent of the colony size. SEM-EBSD characterization of the bi-lamellar microstructures at interrupted tensile strains clarified that deformation behaviors of the bi-lamellar microstructures after yielding were mainly controlled by micro-shear bands across transformed β regions, which eventually evolved into micro-cracks at higher tensile strains. It was considered that the strain compatibility accommodated by the differently aligned micro-shear bands formed within different colonies was the main reason for delaying tensile fracture in the bi-lamellar microstructure with the smaller colony size.
采用新型热处理工艺制备Ti-6Al-4V合金,获得高抗拉强度和大塑性的双片层组织
在本研究中,设计了一种新的通过-β-跨晶处理和临界间退火的方法,使Ti-6Al-4V合金获得了具有细化集落尺寸的双片层组织,从而显著提高了抗拉强度和塑性。通过-β-横贯加工获得的菌落尺寸为60 μm,远小于常规β加工获得的最小菌落尺寸130 μm。集落细化是由于晶界α相的尺寸减小,晶体取向的多样性增加,这是后续集落结构的成核位点。通过对α+β两相区片层组织进行临界间退火并进行水淬处理,得到了由初级α片层组成的双片层组织和由细小次级α板组成的转变β区,并保持了与片层前体相同的集落大小。随着集落尺寸的减小,双片层组织的总伸长率从3.4%提高到18.6%,而高屈服和抗拉强度与集落尺寸无关。SEM-EBSD表征表明,屈服后双层组织的变形行为主要受转变β区的微剪切带控制,并最终在更高的拉伸应变下演变为微裂纹。认为不同菌落内形成的不同排列的微剪切带所适应的应变相容性是导致小菌落双层微观组织延迟拉伸断裂的主要原因。
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