Soft magnetic properties of Fe-B prepared by mechanical alloying

L. Giri, Anit K. Giri, J.M. González
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引用次数: 5

Abstract

Fe100 − xBx (with x = 20, 25 and 50) samples were prepared by high energy ball milling. The phase distribution, thermal stability, saturation magnetization and coercive force of these samples were examined by means of X-ray diffraction, differential scanning calorimetry and vibrating sample and extraction magnetometries, respectively. An excellent soft magnetic behavior, characterized by coercive forces of the order of 2.5 × 10−5 T, was detected in the case of the Fe50B50 samples milled during times from 150 up to 200 hours. This soft magnetic behavior was correlated to the presence of an amorphous phase in the as-milled sample with composition close to the nominal one.

机械合金化制备Fe-B的软磁性能
采用高能球磨法制备Fe100−xBx (x = 20、25和50)样品。分别用x射线衍射、差示扫描量热法和振动取样萃取磁力计检测了样品的相分布、热稳定性、饱和磁化强度和矫顽力。在150 ~ 200小时的铣削时间内,检测到Fe50B50样品具有优异的软磁行为,其矫顽力为2.5 × 10−5 T。这种软磁行为与研磨样品中非晶相的存在有关,其成分与标称相接近。
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