Synthesis and characterization of copper nanoparticles by chemical reduction method

Umme Thahira Khatoon, G. Nageswara Rao, M. Mohan
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引用次数: 13

Abstract

Copper nanoparticles were synthesized using chemical reduction method by reduction of copper sulphate as a metal precursor and sodium borohydride as reducing agent. The particles are characterized and assessed by UV-Vis spectrometer, SEM-EDS and particle size analysis. SEM-EDS and particle size analysis contributed to the analysis of size, shape and composition of copper nanoparticles. UV-Vis spectrometer contributed to analysis of optical properties of the nanoparticles which showed a 550nm and 800nm copper band. The SEM images are also observed and found to be in agreement with the UV-Vis result, confirming the formation of metallic copper nanoparticles. The average particle size at room temperature was less than 16nm. The sizes of the nanoparticles are more controllable by the chemical reduction method.
化学还原法制备铜纳米颗粒及其表征
以硫酸铜为金属前驱体,硼氢化钠为还原剂,采用化学还原法制备了纳米铜。采用紫外-可见光谱、扫描电镜-能谱仪和粒度分析对颗粒进行了表征和评价。SEM-EDS和粒度分析有助于分析铜纳米颗粒的大小、形状和组成。紫外可见分光光度计对纳米粒子的光学性质进行了分析,发现纳米粒子在550nm和800nm处有铜带。SEM图像与UV-Vis结果一致,证实了金属铜纳米颗粒的形成。室温下的平均粒径小于16nm。通过化学还原法,纳米颗粒的尺寸更易控制。
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