Supercritical CO2 Extraction of Oil from Dried Avocado (Persea Americana Mill.) Fruit Pulp: Oil Yield, Solubility, and the Oil Characteristics

N. Tran, T. Q. Dang
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Abstract

The purpose of this study was to investigate the applicability of supercritical fluid technology for extraction of avocado oil. The dried avocado fruit pulp (Persea americana Mill.) was extracted by using a semi-pilot supercritical extraction system. Effect of several process parameters, such as CO2 flow rate, particle size, pressure and temperature on total oil yield, free fatty acid, peroxide value, total phenolic and total flavonoid content in oil were assessed. Avocado oil was extracted within the range for flow rate of 10 and 15L/h, particle size of 2.0 and 3.0 mm, temperature of 34, 42 and 50 oC and pressure of 15, 20, 25 and 30 MPa. Kinetic curves clearly exhibited three periods of extraction (constant rate, falling rate and diffusion-controlled). Increasing flow rate, pressure, temperature or reducing particle size brought an increase in the oil yield and extraction rate. Overall, after 150 min of extraction, the oil in dried avocado was almost completely extracted. The oil yield by supercritical CO2 method (58.97%) obtained at 50 oC and 30 MPa was higher than that by Soxhlet method (55.83%). An increase in pressure (at constant temperature) brought an increase in free fatty acid values in oil but decrease in peroxide values and total phenolic content. On the other hand, the effect of temperature on those parameters was opposite. The oil by supercritical CO2 method was of better quality than that by Soxhlet method.
超临界CO2萃取干鳄梨油(Persea Americana Mill.)果肉:出油率、溶解度和油特性
本研究的目的是探讨超临界流体技术在牛油果油提取中的适用性。采用半中试超临界萃取系统对鳄梨果肉进行了提取。考察了CO2流量、粒径、压力、温度等工艺参数对油中总油收率、游离脂肪酸、过氧化值、总酚和总黄酮含量的影响。在流量为10 ~ 15L/h,粒径为2.0 ~ 3.0 mm,温度为34、42、50℃,压力为15、20、25、30 MPa的条件下提取牛油果油。动力学曲线显示出三个萃取周期(恒速率、下降速率和扩散控制)。增大流量、压力、温度或减小颗粒尺寸均可提高出油率和提取率。总的来说,经过150分钟的提取,牛油果干中的油几乎完全被提取出来。超临界CO2法在50℃、30 MPa条件下的产油率(58.97%)高于索氏法(55.83%)。压力的增加(在恒温下)使油中的游离脂肪酸值增加,但使过氧化值和总酚含量降低。另一方面,温度对这些参数的影响是相反的。超临界CO2法所得油的质量优于索氏法所得油。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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