Synthesis of Al Thin Films with High Optical Transmittance by DC Magnetron Sputtering Process Parameter Optimization

M. S. Rahman, Heon-Ju Lee, M. A. Uddin, I. M. Rizwanul Fattah, Md. Shafiqul Islam
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Abstract

Nanostructured Al thin film with higher optical transmittance and electrical conductivity has intensive applications in solar cells and optical and microelectronic devices. This experimental-based research study has optimized the DC magnetron sputtering deposition parameters (sputtering power, sputtering current, voltage, and working gas pressure) for Al thin film deposition to obtain the highest optical transmittance and lower sheet resistance. Optical transmittance, surface roughness, film thickness, sheet resistance, grain size, and surface morphology were characterized using UV-vis-NIR spectroscopy, surface profiler, spectroscopic ellipsometry, four-point probe, and FE-SEM, respectively to determine the effects of sputtering process parameters on Al films’ different properties. Experimental investigations reveal that electrical conductivity, surface roughness, grain size, and deposition rate increase with increasing of sputtering power at certain working gas pressure. At the optimized condition (sputtering power 80 W, working gas pressure 5 mTorr, deposition time 5 min and ambient temperature), the relatively higher optical transmittance in visible region 96%, moderate sheet resistance 0.196 ohm/square and lowest average surface roughness 2.86 nm were obtained for Al thin film. After all, this research study will help to understand the best Al film deposition parameters in terms of optical transmittance and electrical conductivity for future research and industrial applications.
直流磁控溅射制备高透光率铝薄膜工艺参数优化
纳米结构铝薄膜具有较高的透光率和导电性,在太阳能电池和光学微电子器件中有着广泛的应用。本实验研究优化了用于Al薄膜沉积的直流磁控溅射沉积参数(溅射功率、溅射电流、电压和工作气体压力),以获得最高的透光率和较低的片阻。采用紫外-可见-近红外光谱、表面轮廓仪、光谱椭偏仪、四点探针和FE-SEM等方法分别对透射率、表面粗糙度、膜厚、片阻、晶粒尺寸和表面形貌进行了表征,以确定溅射工艺参数对铝膜不同性能的影响。实验结果表明,在一定的工作气压下,随着溅射功率的增加,电导率、表面粗糙度、晶粒尺寸和沉积速率均有所增加。在最佳条件下(溅射功率80 W,工作气压5 mTorr,沉积时间5 min,环境温度),铝薄膜的可见光区透光率为96%,片材电阻为0.196欧姆/平方,平均表面粗糙度最低为2.86 nm。总之,本研究将有助于从透光率和电导率方面了解最佳Al膜沉积参数,为未来的研究和工业应用提供依据。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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