Minerals Composition and Characterization of the Hatchery Eggshell Waste Treated with Different Preparation Methods

Ahmad Iskandar Setiyawan, Diah Pratiwi, M. F. Karimy, Safna Fauziah
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Abstract

The preparation process needs to be carried out in the treatment of hatchery waste. The objective of the study was to determine the mineral content and characterization of the eggshell waste after preparation. An experiment was arranged on a completely randomized design (CRD). Preparation treatment consisted of; T1: shell waste watered with distilled water; T2: shell waste soaked in distilled water for 12 h; T3: shell waste soaked in 0.5% NaOH for 720 min; and T4: shell waste boiled at 80°C for 15 min and soaked in 5% H3PO4 for 15 min. The data were analyzed using Analysis of Variance (ANOVA), and if any differences, a Duncan Multiple Range Test (DMRT) post hoc tests were carried out. Composition of proximate and mineral were detected by using X-Ray Fluorescence (XRF). Results indicated that proximate analysis of the dry matter content were T4: 98.98±0.01; T3: 98.58±0.04; T2: 98.75±0.08; and T1: 98.72±0.03. The calcium content of the treatment from the highest was T3: 24.22±0.31; T1: 22.80±0.57; T2: 22.77±0.71; and T4: 21.55±0.46. It may be inferred that the treatment technique had no major impact on the eggshells physical characteristics. However, boiling treatment at 80°C for 15 min and soaking in 5% H3PO4 reduced the eggshell waste's Mg, Si, and Ca content. The addition of 0.5% NaOH immersion did not degrade Mg, Ca, and Si of eggshell waste.
不同制备方法处理孵化场蛋壳废弃物的矿物组成及性质
制备过程需要在孵化场废弃物处理中进行。本研究的目的是测定制备后蛋壳废料的矿物含量和性质。试验采用完全随机设计(CRD)。准备处理包括;T1:用蒸馏水浇灌的贝壳废弃物;T2:在蒸馏水中浸泡12 h的贝壳废弃物;T3:贝壳废弃物0.5% NaOH浸泡720 min;T4:壳废物在80°C煮沸15 min,在5% H3PO4中浸泡15 min。数据采用方差分析(ANOVA)进行分析,如有差异,采用Duncan多元极差检验(DMRT)事后检验。用x射线荧光(XRF)测定了其近物和矿物的组成。结果表明:干物质含量近似分析为T4: 98.98±0.01;T3: 98.58±0.04;T2: 98.75±0.08;T1: 98.72±0.03。钙含量从T3处理开始最高:24.22±0.31;T1: 22.80±0.57;T2: 22.77±0.71;T4: 21.55±0.46。由此可以推断,处理工艺对蛋壳的物理特性影响不大。80℃沸煮处理15 min, 5% H3PO4浸泡后,蛋壳渣中Mg、Si、Ca含量降低。0.5% NaOH浸液对蛋壳渣中的镁、钙、硅没有降解作用。
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24 weeks
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