HERBAL SYNTHESIS OF IRON DOPED COBALT OXIDE NANOPARTICLE AND ITS APPLICATIONS

J. J. Priya, C. Duraivathi, J. Poongodi, K. Amudhavalli
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Abstract

Iron doped cobalt oxide nanoparticles were prepared by using Eclipta alba leaves extract. The structural, optical and phase analysis of the synthesized nanoparticles are investigated by X-Ray Diffraction (XRD), Ultraviolet Visible Spectroscopy (UV), and Fourier Transform Infrared Spectroscopy (FTIR) respectively. Scanning Electron microscope (SEM), Energy Dispersive X-Ray Spectroscopy (EDX) and Dynamic Light Scattering (DLS) are used to study the surface morphological, elemental analysis and the hydrodynamic size of the prepared nanoparticles. Methylene Blue (MB) and Congo Red (CR) dye degradation efficacy of the iron doped cobalt oxide nanoparticles are examined using UV. Antibacterial activity for three different bacteria was done using disc diffusion method. Capacitative property of FeCo2O4 was proved by Cyclic Voltammetry (CV) analysis. Thermodynamic properties of the herbal synthesized particle were investigated using Ultrasonic technique using propylene glycol as a base fluid.
草药合成铁掺杂氧化钴纳米颗粒及其应用
以白草叶提取物为原料制备了铁掺杂氧化钴纳米颗粒。利用x射线衍射(XRD)、紫外可见光谱(UV)和傅里叶变换红外光谱(FTIR)对合成的纳米颗粒进行了结构、光学和物相分析。利用扫描电子显微镜(SEM)、能量色散x射线能谱(EDX)和动态光散射(DLS)对制备的纳米颗粒的表面形貌、元素分析和水动力尺寸进行了研究。采用紫外分光光度法考察了铁掺杂氧化钴纳米颗粒对亚甲基蓝(MB)和刚果红(CR)染料的降解效果。采用圆盘扩散法对三种不同细菌进行抑菌活性测定。循环伏安法(CV)证实了FeCo2O4的电容性。以丙二醇为基液,采用超声波技术对合成的草药颗粒的热力学性质进行了研究。
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