Microstructure and Mechanical Property of 14Cr-ODS Ferritic Alloy Produced by Spark Plasma Sintering

Zhengyuan Li, Lu Zheng, Chunmimg Liu
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Abstract

Oxide dispersion strengthened (ODS) ferritic alloys are the leading candidate materials for the advanced fission and fusion reactor due to their excellent radiation tolerance and mechanical properties. These promising performances rely strongly on the high density of nanoscale oxides in ODS alloys. A 14Cr-ODS alloy of Fe-14Cr-2W-0.3Ti-0.3Y2O3 was processed using a combined processing route of mechanical alloy (MA) and spark plasma sintering (SPS). The microstructures of 14Cr-ODS alloy were characterized by using electron backscattered diffraction (EBSD) and transmission electron microscopy (TEM). The results showed that ultrafine grains and high-density nanoscale Y-Ti-O oxides are formed in the 14Cr-ODS alloy. The room temperature tensile strength of 14Cr-ODS alloy is up to 1493 MPa.
放电等离子烧结14Cr-ODS铁素体合金的组织与力学性能
氧化物弥散强化(ODS)铁素体合金因其优异的耐辐射性能和力学性能而成为先进裂变和聚变反应堆的首选候选材料。这些有希望的性能在很大程度上依赖于ODS合金中纳米级氧化物的高密度。采用机械合金(MA)和放电等离子烧结(SPS)相结合的工艺路线,制备了Fe-14Cr-2W-0.3Ti-0.3Y2O3的14Cr-ODS合金。采用电子背散射衍射(EBSD)和透射电镜(TEM)对14Cr-ODS合金的显微组织进行了表征。结果表明:14Cr-ODS合金中形成了超细晶粒和高密度的纳米级Y-Ti-O氧化物;14Cr-ODS合金室温抗拉强度可达1493 MPa。
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