{"title":"Facile One-pot Synthesis of Silver Nanoparticles Supported on α-Zirconium Phosphate Single-Layer Nanosheets","authors":"Jingfang Yu, Luyi Sun","doi":"10.30919/esmm5f223","DOIUrl":null,"url":null,"abstract":"In this paper, we report a facile one-pot synthesis method to prepare well dispersed silver nanoparticles (NPs) supported on α -zirconium phosphate ( α- ZrP) single-layer nanosheets. Silver NPs with a narrow size distribution were reduced on α- ZrP single-layer nanosheet surface due to the electrostatic attractions between the positively charged silver cations and the negatively charged α- ZrP nanosheet support. Three + reducing agents: glucose, NaBH , and tri-sodium citrate were used to reduce Ag . Transmission electron micrographs show that the reduced 4 silver NPs were well dispersed with a diameter of 18.3 ± 4.4 nm, 48.9 ± 13.8 nm, and 3.5 ± 1.0 nm when reduced by glucose, NaBH , and tri- 4 sodium citrate, respectively. Overall, we present a facile method to synthesize Ag NPs with various dimensions for widespread applications.","PeriodicalId":11851,"journal":{"name":"ES Materials & Manufacturing","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2019-05-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"19","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"ES Materials & Manufacturing","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30919/esmm5f223","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 19
Abstract
In this paper, we report a facile one-pot synthesis method to prepare well dispersed silver nanoparticles (NPs) supported on α -zirconium phosphate ( α- ZrP) single-layer nanosheets. Silver NPs with a narrow size distribution were reduced on α- ZrP single-layer nanosheet surface due to the electrostatic attractions between the positively charged silver cations and the negatively charged α- ZrP nanosheet support. Three + reducing agents: glucose, NaBH , and tri-sodium citrate were used to reduce Ag . Transmission electron micrographs show that the reduced 4 silver NPs were well dispersed with a diameter of 18.3 ± 4.4 nm, 48.9 ± 13.8 nm, and 3.5 ± 1.0 nm when reduced by glucose, NaBH , and tri- 4 sodium citrate, respectively. Overall, we present a facile method to synthesize Ag NPs with various dimensions for widespread applications.