Microstructure and magnetic properties of iron-aluminum multilayers

M Carbucicchio , C Grazzi , M Rateo , G Ruggiero , G Turilli
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引用次数: 5

Abstract

Thin film multilayers, constituted by ten Fe/Al bilayers with Fe thickness in the range 15 ÷ 30 Å and constant Al thickness of 20 Å, have been obtained by electron beam evaporation in ultra high vacuum. Sample characterization was performed using transmission electron microscopy, surface Mössbauer spectroscopy and alternating gradient force magnetometry. For iron thickness ≥ 20 Å the periodicity of multilayers is maintained, while for 15 Å the periodicity is almost completely lost and fine particles showing a superparamagnetic behavior begin to form. In all samples the magnetization is laying in the film plane, and, moreover, it shows an easy and hard direction at 90°. The magnetic behavior is typical of poly-domain systems.

铁铝多层膜的微观结构和磁性能
采用超高真空电子束蒸发法制备了10层Fe/Al双层膜,Fe厚度为15 ~ 30 Å, Al厚度为20 ~ Å。采用透射电子显微镜、表面Mössbauer光谱和交变梯度力磁强计对样品进行表征。当铁厚度≥20 Å时,多层膜的周期性保持不变,而当铁厚度≥15 Å时,多层膜的周期性几乎完全丧失,并开始形成具有超顺磁性的细颗粒。在所有样品中,磁化均分布在薄膜平面上,且呈现出90°的易、硬方向。磁性行为是多畴体系的典型特征。
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