Investigation of the effect of different experimental acid solutions applied on the zirconia surface on the bond strength between zirconia and resin cement: A pilot study

IF 0.2 Q4 DENTISTRY, ORAL SURGERY & MEDICINE
Tuba Yılmaz Savaş, A. Savaş, Ceyda Akın, A. Tunçdemir
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Abstract

Aim: The purpose of this study is to examine the effects of two different experimental acid solutions and sandblasting on the bond strength between zirconia ceramic core material and resin cement. Methodology: Forty zirconia core materials were prepared and separated into four groups based on the surface treatment to be applied (n = 10) as follows: 1) Control Group: no surface treatment was performed; 2) Sandblasting Group: the specimen surfaces were sandblasted with 50 µm aluminum oxide particles from a distance of 10 mm at 3 bar pressure for 15 seconds; 3) Sol-1 Group: H2O:HF:H2O2 solution was applied for 60 seconds, washed, and then dried; and 4) Sol-2 Group: H2O:HF:HNO3 solution was applied to the surfaces of the specimens for 60 seconds, washed, and then dried. All specimens were coated with a dual-cure resin cement with a 2.8-mm diameter. After 24 hours, the specimens were tested for shear bond strength (SBS) at 1 mm/min using a universal testing device. Statistical analysis was conducted using one-way analysis of variance (ANOVA) and Tukey HSD tests with a confidence interval of 95%. Results: The difference among the groups was statistically significant (p = 0.002) based on the one-way ANOVA results. The Control Group had the lowest SBS (8.06 ± 4.52), whereas the Sol-1 Group had the highest SBS (17.10 ± 5.67). The Sol-1 and Sol-2 Groups demonstrated comparable bonding strength values (p = 0.17). The Sandblasting and Sol-1 Groups exhibited considerably stronger bond strength than the Control Group (p = 0.05). Conclusion: The experimental acid solutions enhanced the bond strength between the resin cement and the zirconia ceramic at the sandblasting treatment level.   How to cite this article: Yılmaz Savaş T, Savaş A, Akın C, Tunçdemir AR. Investigation of the effect of different experimental acid solutions applied on the zirconia surface on the bond strength between zirconia and resin cement: A pilot study. Int Dent Res 2022;12(Suppl.1):69-73. https://doi.org/10.5577/intdentres.458   Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.
氧化锆表面不同酸溶液对氧化锆与树脂水泥粘结强度影响的初步研究
目的:研究两种不同酸溶液和喷砂对氧化锆陶瓷芯材与树脂水泥粘结强度的影响。方法:制备40种氧化锆芯材,根据表面处理的不同分为4组(n = 10): 1)对照组:不进行表面处理;2)喷砂组:在3 bar压力下,用50µm的氧化铝颗粒从10 mm的距离喷砂15秒;3) Sol-1组:H2O:HF:H2O2溶液作用60秒,洗涤后干燥;4)将Sol-2组:H2O:HF:HNO3溶液涂于标本表面60秒,清洗后干燥。所有标本均涂覆直径为2.8 mm的双固化树脂水泥。24h后,采用通用试验装置以1mm /min的速度测试试件的剪切粘结强度(SBS)。统计学分析采用单因素方差分析(ANOVA)和Tukey HSD检验,置信区间为95%。结果:经单因素方差分析,两组间差异有统计学意义(p = 0.002)。对照组SBS最低(8.06±4.52),Sol-1组SBS最高(17.10±5.67)。Sol-1和Sol-2基团的结合强度值相当(p = 0.17)。喷砂组和Sol-1组的粘接强度显著高于对照组(p = 0.05)。结论:实验酸溶液在喷砂处理水平上增强了树脂水泥与氧化锆陶瓷的粘结强度。本文引用方式:Yılmaz savaki T, savaki A, Akın C, tundemir AR.氧化锆表面不同酸溶液对氧化锆与树脂水泥粘结强度影响的初步研究。国际医学杂志,2022;12(增刊1):69-73。https://doi.org/10.5577/intdentres.458语言修改:本手稿中的英语已由至少两名专业编辑检查,他们都是英语母语者。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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