S. J. Joseph, K. Ranganathan, R. Suresh, R. Arulkumaran, R. Sundararajan, D. Kamalakkannan, S. P. Sakthinathan, G. Vanangamudi, S. Dineshkumar, K. Thirumurthy, I. Muthuvel, G. Thirunarayanan, K. Viveksarathi
{"title":"Synthesis, Characterization and Synthetic Applications of Fly-ash:H3PO4 Nanocatalyst","authors":"S. J. Joseph, K. Ranganathan, R. Suresh, R. Arulkumaran, R. Sundararajan, D. Kamalakkannan, S. P. Sakthinathan, G. Vanangamudi, S. Dineshkumar, K. Thirumurthy, I. Muthuvel, G. Thirunarayanan, K. Viveksarathi","doi":"10.1515/msac-2017-0002","DOIUrl":null,"url":null,"abstract":"Abstract The solid acidic nanocatalyst fly-ash:H3PO4 was prepared and characterized by FT-IR, SEM, EDS and TEM analysis. This catalyst was utilized for aldol condensation, coupling and cyclization reaction. The effect of catalytic activity of this fly-ash:H3PO4 nanocatalyst was studied with the obtained yield of products under solvent-free conditions. In this synthetic reaction the obtained yields were more than 95 %.","PeriodicalId":18239,"journal":{"name":"Materials Science and Applied Chemistry","volume":"88 1","pages":"12 - 20"},"PeriodicalIF":0.0000,"publicationDate":"2017-05-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"4","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/msac-2017-0002","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 4
Abstract
Abstract The solid acidic nanocatalyst fly-ash:H3PO4 was prepared and characterized by FT-IR, SEM, EDS and TEM analysis. This catalyst was utilized for aldol condensation, coupling and cyclization reaction. The effect of catalytic activity of this fly-ash:H3PO4 nanocatalyst was studied with the obtained yield of products under solvent-free conditions. In this synthetic reaction the obtained yields were more than 95 %.