Structure Features of Surface Layers in Structural Steel after Laser-Plasma Alloying with 48(WC–W2 C) + 48Cr + 4Al Powder

O. Berdnikova, O. Kushnarova, A. Bernatskyi, Y. Polovetskyi, V. Kostin, M. Khokhlov
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引用次数: 3

Abstract

The article presents the results of studying the surface layers of structural steel samples alloyed with 48(WC–W2 C) + 48Cr + 4Al powder materials mixture using laser-plasma alloying technology. ROFIN-SINAR Nd:YAG-laser DY044 (Germany) with irradiation wave length λ = 1.06 μm was used for laser alloying. Equipment and technologies of laser-plasma alloying were developed at the E.O. Paton Electric Welding Institute. Detailed studies at all structural levels of grain, subgrain, dislocation structures, including phase precipitates and their stoichiometric composition, were carried out using optical, scanning electron, and microdiffraction transmission electron microscopy. It was found that the formation of crack concentrators in the treated surfaces is due to such structural factors as coarse-grained structure, chemical inhomogeneity, and the formation of dislocation density gradients in grain-boundary areas. Under the optimal mode of laser-plasma alloying of the treated surfaces, a fine-grained structure is formed with a uniform distribution of the dislocation density. In this case, the dislocation substructure is characterized by a cellular type with a cell size of 50…110 nm and by the presence of dispersed phase precipitates up to 100 nm in size in the internal volumes of grains. Dispersion of the structure, the formation of a non-disoriented cellular dislocation substructure with a uniform distribution of dislocation density, the presence of dispersed phase precipitates (nanoscale type) will contribute to an increase in crack resistance and strength characteristics due to substructural and dispersion hardening.
48(wc - w2c) + 48Cr + 4Al粉末激光等离子体合金化后结构钢表层的组织特征
本文介绍了用激光等离子体合金化技术对48(wc - w2c) + 48Cr + 4Al粉末混合材料合金化结构钢试样表层的研究结果。采用辐照波长λ = 1.06 μm的德国ROFIN-SINAR Nd: yag激光DY044进行激光合金化。激光等离子体合金化的设备和技术是由E.O.帕顿电焊研究所开发的。使用光学、扫描电子和微衍射透射电子显微镜对晶粒、亚晶粒、位错结构的所有结构水平进行了详细的研究,包括相沉淀及其化学计量组成。结果表明,裂纹集中剂的形成是由粗晶组织、化学不均匀性和晶界区位错密度梯度等组织因素共同作用的结果。在激光等离子体合金化的最佳模式下,处理后的表面形成了位错密度分布均匀的细晶组织。在这种情况下,位错亚结构的特征是细胞类型,细胞大小为50…110 nm,并且在晶粒内部体积中存在高达100 nm的分散相沉淀。分散的结构,形成具有均匀位错密度分布的非定向胞状位错亚结构,分散相沉淀(纳米级)的存在,由于亚结构和分散硬化,将有助于提高抗裂性和强度特性。
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