Effects of N-Vinylcaprolactam Containing Polyacids and Zirconia on Mechanical Properties of Commercial Glass Ionomer Cements

Shabnam Aslani, H. Rezaie, A. Khavandi
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Abstract

This study aimed to investigate the impact of N-vinylcaprolactam (NVC) and Nano-sized yttria-stabilized zirconia (YSZ), separately and simultaneously, on the mechanical properties of the commercial glass ionomer cements (GICs). Methods: The NVC is able to ameliorate the mechanical and surface properties of glass ionomers; however, its effect hasn’t been investigated in conjunction with zirconia yet. In order to perform the current research, the liquid of glass ionomer was synthesized by adding the NVC to its copolymer and then was characterized by proton nuclear magnetic resonance and Fourier transforms infrared. In addition, Nano-sized YSZ was added to the powder of glass ionomer and then was characterized by scanning electron microscopy. Afterward, the specimens for both flexural strength (FS) and microhardness were prepared by mixing the powder and liquid of the modified glass ionomer. Eventually, the aforementioned properties were evaluated after 24 h and 1 week of immersion in distilled water in an incubator. Furthermore, the one-way analysis of variance was used to study the statistical significance of FS. Results: The obtained results demonstrated that microhardness andFS properties of the glass ionomer were clearly improved as zirconia and NVC were added to the powder and liquid of the glass ionomer, respectively (P<0.05). Moreover, the best result was achieved for the group in which the modification of powder and liquid of glass ionomer occurred concurrently. Conclusion: Based on the findings of the present study, it was deduced that the modified GIC is a promising dental material with improved mechanical properties.
含聚酸和氧化锆的n -乙烯基己内酰胺对商用玻璃离子水泥力学性能的影响
本研究旨在研究n -乙烯基己内酰胺(NVC)和纳米氧化钇稳定氧化锆(YSZ)分别和同时对工业玻璃离子水合物(GICs)力学性能的影响。方法:NVC能改善玻璃离子单体的机械性能和表面性能;然而,它的效果尚未与氧化锆结合研究。为了进行目前的研究,在玻璃离聚体的共聚物中加入NVC合成了玻璃离聚体的液体,并用质子核磁共振和傅里叶变换红外对其进行了表征。此外,将纳米YSZ加入到玻璃离聚体粉末中,并用扫描电镜对其进行了表征。然后,将改性玻璃离子单体的粉末与液体混合制备抗弯强度(FS)和显微硬度试样。最后,在培养箱中蒸馏水浸泡24小时和1周后,评估上述性能。此外,采用单因素方差分析研究FS的统计学意义。结果:得到的结果表明,在玻璃离聚体的粉末和液体中分别添加氧化锆和NVC,可以明显提高玻璃离聚体的显微硬度和fs性能(P<0.05)。同时对玻璃离子单体的粉体和液体进行改性的组效果最好。结论:基于本研究结果,认为改性GIC是一种具有良好力学性能的牙科材料。
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