Comaprison of Iron Nanowires Fabricated via Porous Anodic Aluminium Oxide Template by a.c and d.c. Electrodeposition

Prabhjot Kaur, Sangeeta Sharma, M. Kushwaha
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引用次数: 0

Abstract

In present study nanowires of iron were fabricated by both alternate current (a.c) and direct current (d.c) by using nanoporous anodized aluminium as a template. Nanowires in anodic alumina template were fabricated by electrodeposition method. It has been investigated that synthesis of nanowires is possible by using both a.c and d.c electrodeposition. The nanowires obtained by using a.c electrodeposition were elongated and more stable where as nanowires fabricated by using d.c electrodeposition were less stable. Optimum time attained for the synthesis of nanowires in a.c depostion was 5 minutes where as in case of d.c deposition nanocrystals of different shapes were obtained due to less stability. Average diameter of nanopores obtained in anodized aluminium was 150 nm by using phosphoric acid as a electrolyte. Length of nanowires obtained by using a.c and d.c electrodeposition was 683 nm and 640 nm respectively.
交流与直流电沉积多孔阳极氧化铝模板制备铁纳米线的比较
本研究以纳米多孔阳极氧化铝为模板,采用交流电流和直流电流制备了铁纳米线。采用电沉积法在阳极氧化铝模板中制备纳米线。研究了用交流和直流电沉积法合成纳米线的可能性。采用交流电沉积法制备的纳米线具有较好的延展性和稳定性,而采用直流电沉积法制备的纳米线稳定性较差。在交流沉积中,合成纳米线的最佳时间为5分钟,而在直流沉积中,由于稳定性较差,得到的纳米晶体形状不同。以磷酸为电解液,阳极氧化铝的纳米孔平均直径为150 nm。采用交流电沉积和直流电沉积得到的纳米线长度分别为683nm和640nm。
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