Growth of carbon nanoflakes from nitric acid oxidized electric arc-discharged CNTs and its gas sensing properties

A. Singh
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Abstract

This paper presents synthesis, characterization and gas sensing properties of two dimensional nanostructures i.e. carbon nanoflakes (CNFs) grown by electro-phoretic deposition(EPD) on steel substrate using nitric acid refluxed electric arc synthesized carbon nanotubes(CNTs). Formation of CNFs has been confirmed by XRD and Raman spectra. Optical band gap measurement has been performed by UV-Vis spectroscopy. The morphology of CNFs has been studied via SEM. The EPD film has been characterized for gas sensing. The sensor responded to relatively low concentrations of liquefied petroleum gas (LPG) thus suggesting high-quality CNFs are useful for gas sensors. Sensor has shown maximum response at 200 °C.
硝酸氧化电弧放电碳纳米管的生长及其气敏性能
本文介绍了利用硝酸回流电弧合成的碳纳米管(CNTs)在钢基体上电泳沉积(EPD)生长的二维纳米结构碳纳米片(CNFs)的合成、表征及其气敏性能。通过XRD和拉曼光谱证实了CNFs的形成。用紫外可见光谱法测量了光学带隙。利用扫描电镜对CNFs的形貌进行了研究。EPD薄膜具有气敏特性。该传感器对相对低浓度的液化石油气(LPG)有响应,这表明高质量CNFs对气体传感器很有用。传感器在200°C时显示出最大响应。
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