Influence of Holding Time on Properties of Cemented Carbide- Polycrystalline Diamond Compact Joints

Jia Qianzhong, Li Man, Qu Fuzheng, Z. Hongtao
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Abstract

The influences of brazing holding time on properties of cemented carbide-polycrystalline diamond (PCD) compact joints were investigated in this study. The microstructure and phase composition of joints were investigated by scanning electron microscopy, electron probe microanalyzer, and X-ray diffraction. Microstructural investigations revealed Ag-based solid solution, Cu-based solid solution, Cu0.64Zn0.36, and a small amount of MnNi phase at the joint interface. The max shear strength of brazed joints 350.6 MPa was determined in the samples joined at 15 s, which was partially due to the dispersion strengthening effect of gray-black grains containing Cu-based solid solution, Cu0.64Zn0.36 and MnNi phase in the joints. Equal-area-circle grain diameter of the gray-black grains grew with longer holding time, whereas the shear strength decreased because of the formation of continuous intermetallic compounds layer along the joint boundary. Thermal damage of the PCD layer also deteriorated with increased holding time, and shorter holding time was preferable in the production.
保温时间对硬质合金-聚晶金刚石致密接头性能的影响
研究了钎焊保温时间对硬质合金-聚晶金刚石(PCD)致密接头性能的影响。采用扫描电镜、电子探针显微分析仪和x射线衍射分析了接头的显微组织和相组成。显微组织研究发现,接头界面处存在ag基固溶体、cu基固溶体、Cu0.64Zn0.36和少量MnNi相。15s时钎焊接头的最大抗剪强度为350.6 MPa,部分原因是钎焊接头中含有cu基固溶体、Cu0.64Zn0.36和MnNi相的灰黑色晶粒的弥散强化作用。随着保温时间的延长,灰黑色晶粒的等面积圆晶粒直径增大,但由于沿节理边界形成连续的金属间化合物层,抗剪强度降低。随着保温时间的延长,PCD层的热损伤也随之恶化,在生产中保温时间越短越好。
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