INCORPORATED C70 IN SOL AND GEL

H. Xia, Q. Nie, Jian-li Zhang, Yuepin Zhang
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引用次数: 3

Abstract

C70 is incorporated in gel by a sol-gel process with using 3-amino-propyltriethoxysilane (NH2(CH2)3Si(OC2H5)3, APTS) and 3-glycidoxypropltrimethoxysilane (CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) as precursors. C70 is firstly mixed with APTS to form C70-NH2(CH2)3Si(OC2H5)3 compound by the reaction between C70 and amino-group of APTS, and then the compound is hybridized with GPTMS to form solid gel. The linkage of C70 and APTS is estimated and confirmed with FT-IR spectra, and the UV/Visible spectra of the sol and gel are measured.
在溶胶和凝胶中加入c70
以3-氨基丙基三乙氧基硅烷(NH2(CH2)3Si(OC2H5)3, APTS)和3-甘氧基丙基三甲氧基硅烷(CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS)为前驱体,采用溶胶-凝胶法将C70掺入凝胶中。C70首先与APTS混合,通过C70与APTS的氨基反应生成C70- nh2 (CH2)3Si(OC2H5)3化合物,然后与GPTMS杂交形成固体凝胶。利用FT-IR光谱对C70与APTS的连锁关系进行了估计和确认,并对溶胶和凝胶的紫外/可见光谱进行了测量。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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