Synthesis of Cu2-x Ni0.05 S (x=0.05,0.25,0.30) Compounds and Study of Single Crystals

Kh. Kh. Hashimov
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Abstract

In the article, considering the research studies of many scientists and also on the basis of practical applications, the distribution diagram of copper and sulfur atoms in the phase lattice of the  crystal, the structure transformation diagram, the elemental lattice hexagonal  and  crystallographic data were examined and important results were obtained. Analysis of the studies performed shows that some conflicting results in roentgenographic studies on these compounds are related to obtaining these samples by different methods. Our goal is to obtain single crystals of the compounds Cu2-xNi0.05S (x=0.05,0.25,0.30) and draw the lauegrams and debayograms of those crystals. Then the results were analyzed. During the research, it was found that it is possible to buy single crystals of  compounds based on the analysis of existing methods and selection of the optimal method. As a result of the research, the suitable lauegrams of the single crystals obtained by the Bridgman method and the microstructures of the samples were determined and the possibilities of application were determined.
Cu2-x Ni0.05 S (x=0.05,0.25,0.30)化合物的合成及单晶研究
本文结合许多科学家的研究成果,并结合实际应用,对晶体中铜、硫原子在相点阵中的分布图、结构转变图、元素点阵六角形和晶体学数据进行了检验,得到了重要的结果。对所进行的研究的分析表明,在这些化合物的x线摄影研究中,一些相互矛盾的结果与使用不同的方法获得这些样品有关。我们的目标是得到化合物Cu2-xNi0.05S (x=0.05,0.25,0.30)的单晶,并画出这些晶体的失重图和debal图。然后对结果进行分析。在研究过程中,通过对现有方法的分析和最佳方法的选择,发现购买化合物单晶是可能的。研究结果确定了用Bridgman法获得的单晶的合适分子量和样品的微观结构,并确定了应用的可能性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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