Development of technology for preparation of pressed beet pulp for pectin extraction

N. Daisheva, S. Semenikhin, A. Fabritskaya, M. Usmanov
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Abstract

The growing demand for pectin in food, pharmaceutical and cosmetic industries requires  the search for raw materials for its production and the development of innovative, environmentally  friendly and cost-effective ways to obtain it. A secondary resource of sugar beet processing – pressed  beet pulp which is formed in significant volumes at the sugar beet factories of the Russian Federation can  serve as promising source pectin. At present, the growth of scientific and technological progress has led  to the prospect of using such methods of controlled transformation of plant materials, in which the impact  on the quality and yield of the target component is minimal, in contrast to the classical acid-ethanol  method for producing pectin. Of greatest interest are biotechnological methods for extracting biologically  active substances from plant materials, which provide a higher yield while maintaining their properties.  However, to ensure the maximum effect, it is necessary to prepare plant materials for extraction, since  biotechnological methods have a point focus, as a result of which, under suboptimal conditions, the  efficiency of extracting biologically active substances will be reduced. The aim of the research is to  develop a technology for the preparation of pressed beet pulp using chemical and physical impact methods  for the subsequent process of biotechnological extraction of pectin. To achieve this aim, the pressed beet  pulp treatment with an aqueous solution of hydrogen peroxide has been used as a chemical impact  method, and grinding of pressed beet pulp and its treatment with microwave electromagnetic field (MV  EMF) has been used as physical impact method. Effective technological regimes for the preparation of  pressed beet pulp for pectin extraction using chemical and physical impact methods have been  determined, namely, treatment of pressed beet pulp with a 20% aqueous solution at a ratio of pressed beet  pulp: hydrogen peroxide solution equal to 1,0: 1,0, and constant stirring for 90 minutes, separating the  pulp from the liquid phase, its subsequent grinding to a particle size of less than 2.0 mm and EMF MV  treating with a heating rate to reach a temperature of 60℃, equal to 0,6℃/s. The technology has been  developed for preparing pressed beet pulp for pectin extraction, providing a degree of pectin extraction  of 12,78% to its initial content in pressed beet pulp, which is 10,39% higher compared to the control  (without grinding and treating).
压榨甜菜果肉提取果胶的制备工艺研究
食品、制药和化妆品行业对果胶的需求不断增长,这就要求寻找生产果胶的原料,并开发创新、环保和具有成本效益的方法来获取果胶。甜菜加工的第二种资源-压榨的甜菜浆,在俄罗斯联邦的甜菜工厂中形成了大量的甜菜浆,可以作为有前途的果胶来源。目前,随着科技进步的发展,这种对植物材料进行可控转化的方法具有广阔的应用前景,与传统的酸-乙醇法生产果胶相比,这种方法对目标组分的质量和收率影响最小。人们最感兴趣的是从植物材料中提取生物活性物质的生物技术方法,这种方法在保持其特性的同时提供更高的产量。然而,为了确保最大的效果,必须准备植物材料进行提取,因为生物技术方法有一个点焦点,因此,在次优条件下,提取生物活性物质的效率会降低。本研究的目的是开发一种利用化学和物理冲击方法制备压榨甜菜果肉的技术,为后续的生物技术提取果胶提供技术支持。为达到这一目的,采用双氧水溶液对甜菜压榨浆进行化学冲击处理,采用微波电磁场(MV EMF)对甜菜压榨浆进行研磨和处理作为物理冲击处理。已经确定了利用化学和物理冲击方法制备用于提取果胶的压榨甜菜纸浆的有效技术制度,即用20%的水溶液处理压榨甜菜纸浆,压榨甜菜纸浆与过氧化氢溶液的比例等于1,0:1、0、连续搅拌90分钟,将矿浆从液相中分离出来,随后将其研磨至粒径小于2.0 mm,并以升温速率进行EMF MV处理,温度达到60℃,等于0.6℃/s。开发了用于提取果胶的压榨甜菜纸浆制备技术,其果胶提取率为压榨甜菜纸浆初始含量的12.78%,比对照(未经研磨和处理)高出10.39%。
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