Structure and Surface Texture Characterisation of Fibres and Nanoparticles in Silver(I):6-Guanosine Hydrogel

Lamia L. G. Al-mahamad
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引用次数: 1

Abstract

In this work, silver nanoparticles (AgNPs) have been synthesised via friendly method without adding any reducing agents or exposure to artificial light such as a UV lamp. The method is based on preparing highly stable silver(I):guanosine hydrogel with stoichiometry 1:1. None of monovalent cations were used in this method to induce the formation of the hydrogel. Transmission electron microscopy (TEM) and atomic force microscopy (AFM) techniques were used to investigate the morphology of the formed gel. X-ray diffraction analysis was carried out using the Rietveld method. In addition, surface texture analysis of the self-assembled polymer of silver(I) hydrogel and the silver nanoparticles, that in situ formed in the hydrogel, was carried out.
银- 6-鸟苷水凝胶中纤维和纳米颗粒的结构和表面纹理表征
在这项工作中,银纳米颗粒(AgNPs)已经通过友好的方法合成,而不添加任何还原剂或暴露于人造光(如紫外线灯)。该方法以制备高度稳定的鸟苷银水凝胶为基础,化学计量比为1:1。该方法不使用任何一价阳离子来诱导水凝胶的形成。利用透射电子显微镜(TEM)和原子力显微镜(AFM)技术研究了形成的凝胶的形貌。采用Rietveld法进行x射线衍射分析。此外,还对银(I)水凝胶的自组装聚合物和在水凝胶中原位形成的银纳米粒子进行了表面结构分析。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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