Approaches to rational development of analytical methods for mineral raw materials and products of their processing

B. A. Ovezov
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Abstract

Background. Russia occupies a leading position in the global extraction of minerals, meeting all the demands of Russian economy. The efficiency of resources development determines the efficiency of both the oil and gas industry, as well as related economic sectors. At any stage, geological prospecting and exploration works are carried out sequentially and assume identification of the quantity, quality, shape and size of the valuable component contained in the deposit. In Russia, the recent trend in the development of laboratory research methods consists in creating and implementing hardware approaches capable of identifying the content of valuable components rapidly and accurately.Aim. To compare the existing approaches for obtaining the proportionality coefficient depending on the specifics of the ore deposit under exploration and to analyze the dependence of the amount of laser sampling of microprobes on the relative standard error of sampling the main general sample.Materials and methods. The Richards–Chechott equation and Demond and Halferdahl works were studied. An analysis of error classes was carried out.Results. The relative standard error of sampling the main general sample was found to decrease with an increase in the number of microsamples (pulses). The number of microprobes of an analytical sample depends on the heterogeneity of the valuable component distribution.Conclusion. An increase in the number of laser sampling of microsamples (pulses) leads to a decrease in the relative standard error of sampling the main general sample. The number of microprobes of an analytical sample depends on the heterogeneity of the valuable component distribution (K, α).
合理发展矿物原料及其加工产品分析方法的途径
背景。俄罗斯在全球矿产开采中处于领先地位,满足了俄罗斯经济的所有需求。资源开发的效率决定着油气行业以及相关经济部门的效率。在任何阶段,地质勘探工作都是依次进行的,并确定矿床中有价值成分的数量、质量、形状和大小。在俄罗斯,实验室研究方法发展的最新趋势包括创建和实施能够快速准确地识别有价值成分内容的硬件方法。根据勘查矿床的具体情况,比较了现有的求得比例系数的方法,分析了微探针激光取样量与主要一般样品取样相对标准误差的关系。材料和方法。研究了Richards-Chechott方程和Demond和Halferdahl的工作。对误差分类进行了分析。随着微样品(脉冲)数量的增加,主一般样品的相对标准误差减小。分析样品的微探针数量取决于有价成分分布的非均质性。随着微样品(脉冲)激光采样次数的增加,对主要一般样品进行采样的相对标准误差减小。分析样品的微探针数量取决于有价组分分布(K, α)的非均质性。
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