SINTESIS TIO2-KAOLIN DAN UJI AKTIVITAS FOTOKATALISIS UNTUK ANTIBAKTERI Escherichia Coli DAN Staphylococcus aureus

Desi Listiani, A. Sapar, A. B. Aritonang
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Abstract

Synthesis of TiO2-kaolinite has been performed using solgel method with titanium tetraisopropoxide (TTIP) as precursor. Synthesis of TiO2-kaolinite by temperature calcination 450 °C for 2 hours to obtain TiO2-kaolinite anatase and then the antibacterial photocatalysis activity of E. coli and S. aureus was performed. Identification of the characteristics TiO2-kaolinite used XRD, SEM, FTIR, and DR-UV. It was found that TiO2-kaolinite has been anatase phase structure with the particle size is 19-103 nm, and have a spheric morphology. Infrared spectra indicate a specific group in wave number 921 cm-1. The antibacterial photocatalysis activity test was performed in liquid media and  measurements by the Optical Density (OD) is using Spectrophotometer UV-Vis at wavelength of 600 nm. The results photocatalysisis activity of TiO2-kaolinite for E.coli, TiO2-kaolinite can kill bacteria occured in the 60th minute, while for S. aureus TiO2-kaolin can kill bacteria occured in the 100th minute. Our results clearly that the TiO2-kaolinite has potential as an antibacterial material in water sterilization.
菌根菌聚合和光化活性测试用于耐菌大肠杆菌和菌根球菌菌
以四异丙醇钛(TTIP)为前驱体,采用溶胶法制备了二氧化钛-高岭石。通过450℃温度煅烧2小时合成tio2 -高岭石,得到tio2 -高岭石锐钛矿,并对大肠杆菌和金黄色葡萄球菌进行抑菌光催化活性测定。采用XRD、SEM、FTIR、DR-UV等方法对tio2 -高岭石进行了表征。结果表明:tio2 -高岭石为锐钛矿相结构,粒径为19 ~ 103 nm,具有球形形貌;红外光谱显示波数为921 cm-1的特定基团。在液体介质中进行抗菌光催化活性测试,光密度(OD)用紫外可见分光光度计测定,波长为600 nm。结果tio2 -高岭土对大肠杆菌的光催化活性,tio2 -高岭土能杀灭细菌发生在60分钟,而对金黄色葡萄球菌tio2 -高岭土能杀灭细菌发生在100分钟。研究结果表明,二氧化钛-高岭石具有作为水杀菌材料的潜力。
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