A preliminary study on patulin contamination in spirit drinks

IF 2.5 3区农林科学 Q2 CHEMISTRY, APPLIED

Food additives & contaminants. Part B, Surveillance Pub Date : 2022-04-03 DOI:10.1080/19393210.2022.2066191

Ozgur Golge, Emirhan Yenisehirlioglu, B. Kabak

引用次数: 0

Abstract

ABSTRACT A total of 120 spirit drinks and 40 apple juices were collected between 2018 and 2020 in three regions of Turkey and analysed by high-performance liquid chromatography coupled with a photodiode array detector (HPLC-PDA) for the incidence of patulin. The analytical method was successfully validated for both matrices. In 26.7% of apple juice samples, patulin was quantified at levels between 5.8 and 66.4 µg L−1. Only one regulatory level exceedance was identified for apple juice. The mean dietary exposure of the adult population to patulin ranged from 0.083 to 0.091 ng kg−1 bw day−1. With the HPLC-PDA method, patulin was measured in quantifiable concentrations in 11 out of 25 cognac, 5 out of 40 liqueur, and 1 out of 10 whisky samples, up to a level of 42.6 µg/l, whereas all vodka samples were free from patulin. In only one liqueur sample, the presence of patulin could be confirmed with LC-MS/MS, at a level of 8.9 µg L−1.

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酒精饮料中棒曲霉素污染的初步研究

本研究于2018年至2020年在土耳其三个地区共收集了120种烈酒饮料和40种苹果汁，并采用高效液相色谱-光电二极管阵列检测器(HPLC-PDA)对展霉素的发生率进行了分析。该分析方法成功地验证了这两种矩阵。在26.7%的苹果汁样品中，展青霉素的定量水平在5.8 ~ 66.4µg L−1之间。苹果汁中只有一个超标。成人对展青霉素的平均膳食暴露量为0.083至0.091 ng kg - 1 bw day - 1。采用HPLC-PDA方法，25个干邑样品中有11个、40个利口酒样品中有5个、10个威士忌样品中有1个样品中有展青霉素的可量化浓度，最高可达42.6 μ g/l，而所有伏特加样品中均不含展青霉素。仅在一个利口酒样品中，LC-MS/MS可以确认展霉素的存在，其含量为8.9 μ g L−1。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Food additives & contaminants. Part B, Surveillance 农林科学-毒理学

CiteScore

5.30

自引率

10.30%

发文量

审稿时长

2.7 months

期刊介绍： Food Additives & Contaminants: Part B publishes surveillance data indicating the presence and levels of occurrence of designated food additives, residues and contaminants in foods, food supplements and animal feed. Data using validated methods must meet stipulated quality standards to be acceptable and must be presented in a prescribed format for subsequent data-handling. Food Additives & Contaminants: Part B restricts its scope to include certain classes of food additives, residues and contaminants. This is based on a goal of covering those areas where there is a need to record surveillance data for the purposes of exposure and risk assessment. The scope is initially restricted to: Additives - food colours, artificial sweeteners, and preservatives; Residues – veterinary drug and pesticide residues; Contaminants – metals, mycotoxins, phycotoxins, plant toxins, nitrate/nitrite, PCDDs/PCFDs, PCBs, PAHs, acrylamide, 3-MPCD and contaminants derived from food packaging. Readership: The readership includes scientists involved in all aspects of food safety and quality and particularly those involved in monitoring human exposure to chemicals from the diet. Papers reporting surveillance data in areas other than the above should be submitted to Part A . The scope of Part B will be expanded from time-to-time to ensure inclusion of new areas of concern.