Effect of Neodymium Dopping on Morphology, Phase Changes and Magnetic Properties of Ni0.7Zn0.3NdxFe2-xO4 Ferrite Nanoparticles Synthesized by Complexing Sol-Gel Method
{"title":"Effect of Neodymium Dopping on Morphology, Phase Changes and Magnetic Properties of Ni0.7Zn0.3NdxFe2-xO4 Ferrite Nanoparticles Synthesized by Complexing Sol-Gel Method","authors":"A. Ghasemi, M. L. Estarki, S. Torkian, G. Gordani","doi":"10.47176/jame.39.2.22191","DOIUrl":null,"url":null,"abstract":": The purpose of this study was to evaluate phase changes and magnetic properties of neodymium doped Ni 0.7 Zn 0.3 Nd x Fe 2-x O 4 (x = 0, 0.01, 0.03, 0.05, 0.07, 0.10) nanoparticles synthesized by complexing sol-gel method. In this method, triethanolamine (TEA) acted as both a gelling agent and a chelating agent. Samples were characterized by X-ray diffraction (XRD) analysis, field emission scanning electron microscopy (FESEM), and energy dispersive X-ray spectroscopy (EDX). XRD patterns of all synthesized samples revealed the formation of a spinel ferrite phase. Magnetic evaluation of the specimens showed that the Nd 0.01 doped sample with a quasi-spherical morphology and particle size of about 60 nm has the highest saturation magnetization of 50 emu/g and coercive force of 103 Oe.","PeriodicalId":30992,"journal":{"name":"Journal of Advanced Materials in Engineering","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2020-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Advanced Materials in Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.47176/jame.39.2.22191","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
: The purpose of this study was to evaluate phase changes and magnetic properties of neodymium doped Ni 0.7 Zn 0.3 Nd x Fe 2-x O 4 (x = 0, 0.01, 0.03, 0.05, 0.07, 0.10) nanoparticles synthesized by complexing sol-gel method. In this method, triethanolamine (TEA) acted as both a gelling agent and a chelating agent. Samples were characterized by X-ray diffraction (XRD) analysis, field emission scanning electron microscopy (FESEM), and energy dispersive X-ray spectroscopy (EDX). XRD patterns of all synthesized samples revealed the formation of a spinel ferrite phase. Magnetic evaluation of the specimens showed that the Nd 0.01 doped sample with a quasi-spherical morphology and particle size of about 60 nm has the highest saturation magnetization of 50 emu/g and coercive force of 103 Oe.