Damage evolution of the coating/substrate system TiN/X2CrNi18-9 under high indentation loads: experimental and numerical study

IF 2.7 3区 材料科学 Q2 ENGINEERING, MECHANICAL
Amir Bahri, Manel Ellouz, Michaela Klöcker, Khaled Elleuch, Thomas Kordisch
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Abstract

Hard coatings, in particular TiN, are widely used as coatings for cutting tools and in the agri-food industry. In the literature, however, few characterizations of hard coatings can be found which define the minimum applied load when the coating starts to fail. In the present study TiN coating was deposited on stainless steel X2CrNi18-9. Vickers and Brinell indentation tests with a wide load range were performed. The main results revealed that the increase of the applied load in Vickers and Brinell indentation influenced the coating and coating/substrate damage evolution. SEM investigation of the Vickers indentation area shows five modes of damage: inclined cracks, radial cracks, lateral cracks, edge cracks, and shear steps. Each damage mode occurs at a specific load range. Parallel cracks already appeared at the edges of the indents at the lowest load of 2 N. For Brinell indentation, cracks start in the coating only at loads higher than F = 307 N. The SEM examinations present damage modes such as circumferential cracks in the border and additional circular cracks in the center of the indent, creating a crack network. Numerical simulations of Brinell indentation were carried out in order to determine the stress distribution in the indent. The comparison of the numerical simulation results with the experimental findings revealed that the coating started to fail at a stress range above 5735 MPa which corresponds to a normal load range of higher than 307 N in Brinell indentation tests. At a load of 613 N cracks were observed.

Abstract Image

高压痕载荷下涂层/基底系统 TiN/X2CrNi18-9 的损伤演变:实验和数值研究
硬涂层,特别是 TiN,被广泛用作切削工具和农业食品工业的涂层。然而,在文献中,很少有关于硬涂层特性的研究能确定涂层开始失效时的最小外加载荷。本研究在不锈钢 X2CrNi18-9 上沉积了 TiN 涂层。进行了大载荷范围的维氏和布氏压痕测试。主要结果表明,维氏硬度和布氏压痕中施加载荷的增加会影响涂层和涂层/基体损伤的演变。对维氏硬度压痕区域的扫描电子显微镜调查显示了五种损坏模式:倾斜裂纹、径向裂纹、横向裂纹、边缘裂纹和剪切阶梯。每种损坏模式都出现在特定的载荷范围内。扫描电子显微镜(SEM)的检测结果显示了多种损坏模式,如边缘的圆周裂纹和压痕中心的附加圆形裂纹,从而形成了裂纹网络。为了确定压痕中的应力分布,对布氏压痕进行了数值模拟。将数值模拟结果与实验结果进行比较后发现,涂层在应力范围超过 5735 兆帕时开始失效,这与布氏压痕测试中高于 307 牛顿的正常载荷范围相对应。在 613 N 的载荷下观察到了裂纹。
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来源期刊
International Journal of Mechanics and Materials in Design
International Journal of Mechanics and Materials in Design ENGINEERING, MECHANICAL-MATERIALS SCIENCE, MULTIDISCIPLINARY
CiteScore
6.00
自引率
5.40%
发文量
41
审稿时长
>12 weeks
期刊介绍: It is the objective of this journal to provide an effective medium for the dissemination of recent advances and original works in mechanics and materials'' engineering and their impact on the design process in an integrated, highly focused and coherent format. The goal is to enable mechanical, aeronautical, civil, automotive, biomedical, chemical and nuclear engineers, researchers and scientists to keep abreast of recent developments and exchange ideas on a number of topics relating to the use of mechanics and materials in design. Analytical synopsis of contents: The following non-exhaustive list is considered to be within the scope of the International Journal of Mechanics and Materials in Design: Intelligent Design: Nano-engineering and Nano-science in Design; Smart Materials and Adaptive Structures in Design; Mechanism(s) Design; Design against Failure; Design for Manufacturing; Design of Ultralight Structures; Design for a Clean Environment; Impact and Crashworthiness; Microelectronic Packaging Systems. Advanced Materials in Design: Newly Engineered Materials; Smart Materials and Adaptive Structures; Micromechanical Modelling of Composites; Damage Characterisation of Advanced/Traditional Materials; Alternative Use of Traditional Materials in Design; Functionally Graded Materials; Failure Analysis: Fatigue and Fracture; Multiscale Modelling Concepts and Methodology; Interfaces, interfacial properties and characterisation. Design Analysis and Optimisation: Shape and Topology Optimisation; Structural Optimisation; Optimisation Algorithms in Design; Nonlinear Mechanics in Design; Novel Numerical Tools in Design; Geometric Modelling and CAD Tools in Design; FEM, BEM and Hybrid Methods; Integrated Computer Aided Design; Computational Failure Analysis; Coupled Thermo-Electro-Mechanical Designs.
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