Rubber (Hevea brasiliensis) Seed shell Activated Carbon Preparation, Characterization and Antibacterial Activity Studies

Q3 Chemistry
S. Samanman, Nuttaporn Tepprom, Inun Yipong, Yasmee Saleah, Kholeeyah Navani, Nifanusi Samae, Amri Hj Mohammed, A. S. Abd Aziz
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Abstract

In Thailand, the rubber tree is widely used as a source of natural rubber and their seeds have been found to be rich in oil production. The seed shell is the residue and not edible but abundantly available in the country. Therefore, the objective of this work was to prepare activated carbon (AC) from rubber seed shells. ACs were produced by chemical activation and their characteristics were investigated. The effects of activation temperature and chemical impregnation time in the agent were examined. Proximate analysis was investigated and the results were within the standard of AC. The adsorption capacity was demonstrated with BET, iodine, and methylene blue number. The best produced AC (700 °C of activation temperature and 24 h of impregnation time) provided the highest BET surface area, iodine and methylene blue number were 923 m2/g, 1,234±24 mg/g and 1,204±10 mg/g, respectively. FT-IR spectrum indicates the presence of oxygen and nitrogen containing surface functional groups such as -OH, -CH3, -CH2, C=C, C-O, and N-H groups. The microstructure of the produced ACs was examined by SEM and the results found that they are porosity. The antibacterial effect results were discovered to be also effective against E. coli and S. aureus after 3 h and 24 h of contact times, respectively. In addition, the prepared AC also provided many properties that are better than those obtained by the commercial AC. Finally, it can be concluded that, AC from rubber seed shell can be applied as a low cost and possible alternate adsorbent.
橡胶籽壳活性炭的制备、表征及抗菌活性研究
在泰国,橡胶树被广泛用作天然橡胶的来源,人们发现它们的种子富含石油。种子外壳是残渣,不可食用,但在该国可大量获得。因此,本工作的目的是从橡胶籽壳中制备活性炭。采用化学活化方法制备了活性炭,并对其特性进行了研究。考察了活化温度和化学浸渍时间对试剂性能的影响。进行了近似分析,结果在AC标准范围内。用BET、碘和亚甲基蓝值证明了吸附能力。最佳生产的AC(700°C的活化温度和24小时的浸渍时间)提供了最高的BET表面积,碘和亚甲蓝值分别为923m2/g、1234±24 mg/g和1204±10 mg/g。FT-IR光谱表明存在含氧和氮的表面官能团,如-OH、-CH3、-CH2、C=C、C-O和N-H基团。通过SEM对所制备的AC的微观结构进行了检查,结果发现它们是多孔的。在接触3小时和24小时后,发现抗菌效果结果对大肠杆菌和金黄色葡萄球菌也分别有效。此外,所制备的AC还提供了许多比商用AC更好的性能。最后,可以得出结论,来自橡胶籽壳的AC可以作为一种低成本和可能的替代吸附剂应用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Molekul
Molekul Chemistry-Chemistry (all)
CiteScore
1.30
自引率
0.00%
发文量
31
审稿时长
4 weeks
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