Synthesis, Spectroscopic, and Thermal Analyses of 2-Oxo-1,2-dihydroquinolin-8-yl 4-chlorobenzoate

IF 0.6 Q4 CHEMISTRY, ORGANIC
Molbank Pub Date : 2023-06-19 DOI:10.3390/m1672
Diana Becerra, Hugo Rojas, J. Castillo
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引用次数: 0

Abstract

The 2-oxo-1,2-dihydroquinolin-8-yl 4-chlorobenzoate was synthesized in good yield using a triethylamine-mediated O-acylation reaction between 8-hydroxyquinolin-2(1H)-one and 4-chlorobenzoyl chloride in acetonitrile at room temperature. This methodology is notable for its clean reaction profile and straightforward procedure. The 2-oxoquinoline derivative was characterized using spectroscopic, spectrometric, and thermal analyses, enabling a comprehensive understanding of its molecular structure and thermal properties.
2-氧-1,2-二氢喹啉-8-酰基4-氯苯甲酸酯的合成、光谱和热分析
采用三乙胺介导的8-羟基喹啉-2(1H)-酮与4-氯苯甲酰氯在乙腈中的O-酰化反应,在室温下合成了2-氧代-1,2-二氢喹啉-8-基4-氯苯甲酸酯。这种方法以其干净的反应曲线和简单的程序而闻名。通过光谱、光谱和热分析对2-氧代喹啉衍生物进行了表征,从而能够全面了解其分子结构和热性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Molbank
Molbank Chemistry-Physical and Theoretical Chemistry
CiteScore
0.70
自引率
33.30%
发文量
174
审稿时长
11 weeks
期刊介绍: •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)
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