Investigation of cycloaliphatic amine-cured bisphenol-A epoxy resin under quenching treatment and the effect on its carbon fiber composite lamination strength

IF 1.7 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
H. Sukanto, W. W. Raharjo, D. Ariawan, J. Triyono
{"title":"Investigation of cycloaliphatic amine-cured bisphenol-A epoxy resin under quenching treatment and the effect on its carbon fiber composite lamination strength","authors":"H. Sukanto, W. W. Raharjo, D. Ariawan, J. Triyono","doi":"10.1515/jmbm-2022-0266","DOIUrl":null,"url":null,"abstract":"Abstract Thermosetting epoxy resin polymer with cycloaliphatic amines curing agent has been widely used for a composite matrix with carbon fiber reinforcement. The utilization was increased due to the superior performance of this epoxy resin compared to other polymers. However, a changing operational environment has potentially reduced composite performance, which most likely begins with matrix degradation. This research applies thermal treatment by the quenching process sequence to the epoxy resin matrix and its reinforced carbon fiber composite (CFRP). The composite is made by epoxy resin diglycidyl ether bisphenol-A, curing with cycloaliphatic amine as matrix and strengthening carbon fiber mat/woven. Three times quenching treatment was performed by heating the specimen around the glass transition temperature and then dipped immediately in fresh water. After quenching treatment, the epoxy resin shows a reduction in tensile strength and elongation. Under infrared observation, epoxy resin does not significantly show changes in functional groups. Investigation under X-ray refraction also indicates no difference in a crystalline structure; this epoxy resin stays in an amorphous form before and after quenching. In contrast to the matrix, the quenching treatment of the CFRP composite above the epoxy resin s glass transition temperature revealed an increase in the interlaminar shear strength (ILSS). The matrix ductility reduction after quenching should be carefully considered for application in the form of epoxy resin sheets or CFRP composite construction materials.","PeriodicalId":17354,"journal":{"name":"Journal of the Mechanical Behavior of Materials","volume":" ","pages":""},"PeriodicalIF":1.7000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Mechanical Behavior of Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/jmbm-2022-0266","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 1

Abstract

Abstract Thermosetting epoxy resin polymer with cycloaliphatic amines curing agent has been widely used for a composite matrix with carbon fiber reinforcement. The utilization was increased due to the superior performance of this epoxy resin compared to other polymers. However, a changing operational environment has potentially reduced composite performance, which most likely begins with matrix degradation. This research applies thermal treatment by the quenching process sequence to the epoxy resin matrix and its reinforced carbon fiber composite (CFRP). The composite is made by epoxy resin diglycidyl ether bisphenol-A, curing with cycloaliphatic amine as matrix and strengthening carbon fiber mat/woven. Three times quenching treatment was performed by heating the specimen around the glass transition temperature and then dipped immediately in fresh water. After quenching treatment, the epoxy resin shows a reduction in tensile strength and elongation. Under infrared observation, epoxy resin does not significantly show changes in functional groups. Investigation under X-ray refraction also indicates no difference in a crystalline structure; this epoxy resin stays in an amorphous form before and after quenching. In contrast to the matrix, the quenching treatment of the CFRP composite above the epoxy resin s glass transition temperature revealed an increase in the interlaminar shear strength (ILSS). The matrix ductility reduction after quenching should be carefully considered for application in the form of epoxy resin sheets or CFRP composite construction materials.
脂环族胺固化双酚A环氧树脂淬火处理及其对碳纤维复合材料层合强度影响的研究
以环脂肪胺为固化剂的热固性环氧树脂聚合物已被广泛应用于碳纤维增强复合材料基体。与其他聚合物相比,该环氧树脂性能优越,提高了利用率。然而,不断变化的操作环境可能会降低复合材料的性能,这很可能从基体退化开始。本研究采用淬火工艺顺序对环氧树脂基体及其增强碳纤维复合材料(CFRP)进行热处理。该复合材料以环氧树脂二缩水甘油酯醚双酚a为基材,以环脂肪胺为基体固化,增强碳纤维垫/编织而成。在玻璃化转变温度附近加热试样,然后立即浸入淡水中进行三次淬火处理。淬火处理后,环氧树脂的抗拉强度和伸长率下降。红外观察环氧树脂的官能团变化不明显。x射线折射研究也表明晶体结构没有差异;这种环氧树脂在淬火前后都保持无定形。与基体相比,在环氧树脂玻璃化转变温度以上淬火处理CFRP复合材料的层间抗剪强度(ILSS)有所提高。以环氧树脂片材或CFRP复合建筑材料的形式应用时,应仔细考虑淬火后基体延展性的降低。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
Journal of the Mechanical Behavior of Materials
Journal of the Mechanical Behavior of Materials Materials Science-Materials Science (miscellaneous)
CiteScore
3.00
自引率
11.10%
发文量
76
审稿时长
30 weeks
期刊介绍: The journal focuses on the micromechanics and nanomechanics of materials, the relationship between structure and mechanical properties, material instabilities and fracture, as well as size effects and length/time scale transitions. Articles on cutting edge theory, simulations and experiments – used as tools for revealing novel material properties and designing new devices for structural, thermo-chemo-mechanical, and opto-electro-mechanical applications – are encouraged. Synthesis/processing and related traditional mechanics/materials science themes are not within the scope of JMBM. The Editorial Board also organizes topical issues on emerging areas by invitation. Topics Metals and Alloys Ceramics and Glasses Soils and Geomaterials Concrete and Cementitious Materials Polymers and Composites Wood and Paper Elastomers and Biomaterials Liquid Crystals and Suspensions Electromagnetic and Optoelectronic Materials High-energy Density Storage Materials Monument Restoration and Cultural Heritage Preservation Materials Nanomaterials Complex and Emerging Materials.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信