Calcium carbonate nanoparticles of quail’s egg shells: Synthesis and characterizations

IF 1.7 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
N. Ahmed, Faten Kamil, Adnan Ali Hasso, A. N. Abduljawaad, Thekra Fadel Saleh, S. Mahmood
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引用次数: 7

Abstract

Abstract Avian eggshell is a natural biomaterial that has been used as an alternative natural source of CaCO3 and is accessible in big amounts from egg manufacturing. This study was planned to estimate CaCO3 in quail’s eggshell because it has a probable use in the progress of a novel choice of many applications. Physical properties: mineralogical documentation of the natural eggshell nanoparticles were approved using XRD and FTIR to explore the chemical bond or molecular structure of the materials. Micrographs were obtained using FESEM/EDX and TEM to identify the morphology and size of nanoparticles. The results showed that quail eggshell was soft, with white to light sand color, and a smooth texture which allows good deposition of different color spots, from black to brown spots. The resulted of eggshells signifies almost 8.4% w/w of the overall weight (12.2) gram of quail egg and 91.60% w/w of the micropowder to the full weight of (0.94) gram of quail eggshell. The results presented that calcium is the main element in an eggshell; frequently occurs in a formula of CaCO3 and the crystal construction was almost pure calcite. FTIR spectra for quail eggshell demonstrated the existence of the out of plane bending, the asymmetric stretching, and the plane bending styles of the carbonate groups, specific of normal dolomite, situated at 873 cm–1, 1405 cm–1, and 710 cm–1, respectively. The FESEM and TEM for nanoparticles were shown calcite CaCO3 nanoparticles with an ordinary size of ≤ 100 nm for FESEM and with a variety size of ≤ 50 nm for TEM. Unfortunately, eggshell is an egg product manufacturing deposit. These incomes will let fast developments in proportional studies of the organic elements of avian eggshell and their purposeful consequences by usages of eggshell in nourishment and medicine which can be applied for many resolutions that diminish their consequence on environmental contamination.
鹌鹑蛋壳的碳酸钙纳米颗粒:合成和表征
禽蛋壳是一种天然生物材料,已被用作CaCO3的替代天然来源,并且可以从鸡蛋制造中大量获取。本研究计划估计鹌鹑蛋壳中的CaCO3,因为它可能在许多应用的新选择的进展中使用。物理性质:利用XRD和FTIR对天然蛋壳纳米颗粒进行了矿物学记录,以探索材料的化学键或分子结构。利用FESEM/EDX和TEM对纳米颗粒的形貌和尺寸进行了表征。结果表明,鹌鹑蛋壳质地柔软,呈白色至浅砂色,质地光滑,适合沉积从黑色到棕色等不同颜色的斑点。结果表明,微粉对鹌鹑蛋壳总重(12.2)g的w/w约占8.4%,对鹌鹑蛋壳总重(0.94)g的w/w约占91.60%。结果表明:钙是蛋壳中的主要元素;经常出现在CaCO3分子式中,晶体结构几乎为纯方解石。鹌鹑壳的FTIR光谱显示,普通白云岩的碳酸盐基团分别位于873 cm-1、1405 cm-1和710 cm-1处,存在平面外弯曲、不对称拉伸和平面弯曲。纳米颗粒的FESEM和TEM显示,方解石CaCO3纳米颗粒,FESEM显示为普通尺寸≤100 nm, TEM显示为各种尺寸≤50 nm。不幸的是,蛋壳是蛋制品的制造沉积物。这些收入将促进对禽蛋壳有机成分的比例研究的快速发展,并通过蛋壳在营养和医药中的使用产生有目的的后果,这些研究可用于许多解决方案,以减少它们对环境污染的影响。
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来源期刊
Journal of the Mechanical Behavior of Materials
Journal of the Mechanical Behavior of Materials Materials Science-Materials Science (miscellaneous)
CiteScore
3.00
自引率
11.10%
发文量
76
审稿时长
30 weeks
期刊介绍: The journal focuses on the micromechanics and nanomechanics of materials, the relationship between structure and mechanical properties, material instabilities and fracture, as well as size effects and length/time scale transitions. Articles on cutting edge theory, simulations and experiments – used as tools for revealing novel material properties and designing new devices for structural, thermo-chemo-mechanical, and opto-electro-mechanical applications – are encouraged. Synthesis/processing and related traditional mechanics/materials science themes are not within the scope of JMBM. The Editorial Board also organizes topical issues on emerging areas by invitation. Topics Metals and Alloys Ceramics and Glasses Soils and Geomaterials Concrete and Cementitious Materials Polymers and Composites Wood and Paper Elastomers and Biomaterials Liquid Crystals and Suspensions Electromagnetic and Optoelectronic Materials High-energy Density Storage Materials Monument Restoration and Cultural Heritage Preservation Materials Nanomaterials Complex and Emerging Materials.
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