Synthesis and Crystal Structure of 1,3-Bis(5-chloro-3-methoxysalicylideneamino)-2-propanol Trihydrate

Abstract

X-ray quality crystals were grown by slow the data collected on a Bruker CCD X-ray diffractometer (SMART APEX) using graphite-monochromated Mo- K α radiation. Crystal data and data Table The structure was solved by an intrinsic phasing method and refined The title compound, 1,3-bis(5-chloro-3-methoxysalicylideneamino)-2-propanol trihydrate, was synthesized and the crystal structure was determined by the single-crystal X-ray diffraction method at 90 K. It crystallizes in the monoclinic space group P 2/ c with a = 18.098(3)Å, b = 4.3275(8)Å, c = 14.572(3)Å, β = 104.283(3) ° , V = 1106.0(3)Å 3 , D x = 1.445 g/cm 3 ,