Microstructure of a new ODS Cu–0.7wt-%Cr–0.11wt-%Zr material produced by a novel powder metallurgical method

IF 1.9 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING
M. Eddahbi, M. Monge, A. Muñoz, Ó. J. Durá, B. Savoini
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引用次数: 1

Abstract

ABSTRACT A new oxide dispersion strengthened Cu–0.7wt-%Cr–0.11wt-%Zr material was processed via mechanical alloying (MA) and hot isostatic pressing (HIP). A fine dispersion of yttria particles (Y2O3) was incorporated to the Cu matrix via the addition of yttrium (III) acetate tetrahydrate (C6H9O6Y·4H2O) powder (Y3ATH), which decomposed during thermomechanical processing and subsequent thermal annealing. The microstructure after consolidation by HIP revealed the coexistence of zones with a low and high density of precipitates/particles, LDPZ and HDPZ, respectively. The HDPZ were characterized by fine grains with an average size of ∼300 nm and fine Y–O rich particles (∼40 nm) and Cr rich coarse particles (∼215 nm), homogenously distributed in the Cu matrix. However, the LDPZ contained coarse grains containing 60°/〈111〉 (Σ3) twins’ boundaries.
新型粉末冶金法制备Cu-0.7wt -% Cr-0.11wt -%Zr ODS材料的显微组织
采用机械合金化(MA)和热等静压(HIP)法制备了一种新型的Cu-0.7wt -% Cr-0.11wt -%Zr氧化物弥散强化材料。通过添加四水合物醋酸钇(III) (C6H9O6Y·4H2O)粉末(Y3ATH),将钇颗粒(Y2O3)分散到Cu基体中,并在热处理和后续热处理过程中分解。HIP固结后的微观结构显示析出相/颗粒密度区LDPZ区和高密度区HDPZ区共存。HDPZ具有平均尺寸为~ 300 nm的细晶粒和均匀分布在Cu基体中的富Y-O细颗粒(~ 40 nm)和富Cr粗颗粒(~ 215 nm)的特征。然而,LDPZ含有含有60°/ < 111 > (Σ3)孪晶界的粗晶。
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来源期刊
Powder Metallurgy
Powder Metallurgy 工程技术-冶金工程
CiteScore
2.90
自引率
7.10%
发文量
30
审稿时长
3 months
期刊介绍: Powder Metallurgy is an international journal publishing peer-reviewed original research on the science and practice of powder metallurgy and particulate technology. Coverage includes metallic particulate materials, PM tool materials, hard materials, composites, and novel powder based materials.
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