DyPO4·1.5H2O Microcrystals: Microwave/Ultrasound/ Ultraviolet Light- Assisted Synthesis, Characterization and Formation Mechanism

IF 0.9 Q4 CHEMISTRY, MULTIDISCIPLINARY
Mengmeng Li, Shuang Huang, Han Zhang, Lei Wang, Shengliang Zhong
{"title":"DyPO4·1.5H2O Microcrystals: Microwave/Ultrasound/ Ultraviolet Light- Assisted Synthesis, Characterization and Formation Mechanism","authors":"Mengmeng Li, Shuang Huang, Han Zhang, Lei Wang, Shengliang Zhong","doi":"10.2174/2213335607666200701214200","DOIUrl":null,"url":null,"abstract":"\n\nResearchers have pursued the new synthesis method. As a newly developed\nmethod, microwave (MW), ultrasound (US) and ultraviolet light (UV) assisted synthesis has drawn\nincreasing interests. Under the synergistic effect, many materials with new structure, morphology and\nproperties may be found. As an important rare-earth phosphate, DyPO4 was selected and the effect of\nMW, US and UV on the preparation was investigated.\n\n\n\nThe DyPO4·1.5H2O nanostructures were prepared by MW, US, UV and their combination.\n\n\n\nHexagonal DyPO4·1.5H2O microcrystals obtained under MW irradiation were broomstick\nbundles. Needle-shaped products were formed in the presence of MW and US. Interestingly, the\nbroom-sheaf-like structures can self-assemble into flower-shaped structures upon the irradiation of\nMW and UV. Whereas, MW/UV/US synergetic heating results in mixed morphologies of flower-like\nand needle-shaped structures.\n\n\n\nThe growth of DyPO4 nanostructures can be tuned by selecting the combination of heating\nmethod of MW, US and UV.\n","PeriodicalId":43539,"journal":{"name":"Current Microwave Chemistry","volume":null,"pages":null},"PeriodicalIF":0.9000,"publicationDate":"2020-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Current Microwave Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2174/2213335607666200701214200","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

Abstract

Researchers have pursued the new synthesis method. As a newly developed method, microwave (MW), ultrasound (US) and ultraviolet light (UV) assisted synthesis has drawn increasing interests. Under the synergistic effect, many materials with new structure, morphology and properties may be found. As an important rare-earth phosphate, DyPO4 was selected and the effect of MW, US and UV on the preparation was investigated. The DyPO4·1.5H2O nanostructures were prepared by MW, US, UV and their combination. Hexagonal DyPO4·1.5H2O microcrystals obtained under MW irradiation were broomstick bundles. Needle-shaped products were formed in the presence of MW and US. Interestingly, the broom-sheaf-like structures can self-assemble into flower-shaped structures upon the irradiation of MW and UV. Whereas, MW/UV/US synergetic heating results in mixed morphologies of flower-like and needle-shaped structures. The growth of DyPO4 nanostructures can be tuned by selecting the combination of heating method of MW, US and UV.
DyPO4·1.5H2O微晶:微波/超声/紫外光辅助合成、表征及形成机理
研究人员一直在探索这种新的合成方法。微波(MW)、超声波(US)和紫外光(UV)辅助合成作为一种新兴的合成方法,越来越受到人们的关注。在协同作用下,可以发现许多具有新结构、新形态和新性能的材料。选择了一种重要的稀土磷酸盐DyPO4,考察了微波、超声和紫外对其制备的影响。采用微波、超声、紫外光谱及其组合方法制备了DyPO4·1.5H2O纳米结构。在微波辐照下获得的六方晶系DyPO4·1.5H2O微晶为扫帚状晶束。在MW和US存在下形成针状产物。有趣的是,在MW和UV的照射下,房间鞘状结构可以自组装成花状结构。然而,MW/UV/US协同加热导致花朵状和针状结构的混合形态。DyPO4纳米结构的生长可以通过选择MW、US和UV加热方法的组合来调节。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
Current Microwave Chemistry
Current Microwave Chemistry CHEMISTRY, MULTIDISCIPLINARY-
自引率
0.00%
发文量
11
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信