Karakteristik Struktur Kristal In2Se3 Hasil Preparasi Dengan Metode Bridgman

Ulikaryani Ulikaryani, Jenal Sodikin, Nur Akhlis Sarihidaya Laksana, Unggul Satria Jati, Ari Kristiningsih
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Abstract

Apart from using silicon material, thin-layer solar cells can be made from various types of semiconductor materials, such as a combination of groups III and VI. In solar cell applications, these materials are usually used as n-type coatings. This study not only aimed to determine the crystal structure and the effect of annealing temperature on the crystal lattice parameters but also to determine the chemical composition and surface morphological structure of the crystals formed from the preparation. The crystal growth process was carried out using the Bridgman method with different heating patterns. The temperature in both annealing temperatures is 200oC and 250oC. The physical properties of the prepared In2Se3 crystals were characterized using XRD, SEM, and EDAX. XRD Characterization was used to determine the crystal structure, while SEM and EDAX characterization was used to determine the surface morphology and chemical composition of the crystals. The result of the XRD characterization showed that the formed In2Se3 crystals were polycrystals with a hexagonal structure. Based on the diffractogram obtained, the In2Se3 crystalline heating 1 has better quality. EDAX analysis showed that the In2Se3 crystals were composed of elements of In and Se with a mole ratio of 2:9, while the SEM characterization showed that the color of the surface morphology of the In2Se3 crystals was not homogeneous.
用布里奇曼方法进行的晶体结构特征
除了使用硅材料外,薄层太阳能电池还可以由各种类型的半导体材料制成,例如III族和VI族的组合。在太阳能电池应用中,这些材料通常用作n型涂层。本研究不仅旨在确定晶体结构和退火温度对晶格参数的影响,还旨在确定制备过程中形成的晶体的化学成分和表面形态结构。采用Bridgman法在不同的加热模式下进行晶体生长。退火温度均为200oC和250oC。采用XRD、SEM和EDAX对制备的In2Se3晶体的物理性质进行了表征。采用XRD表征确定晶体结构,SEM和EDAX表征确定晶体的表面形貌和化学组成。XRD表征结果表明,形成的In2Se3晶体为六边形结构的多晶。从衍射图上可以看出,In2Se3结晶加热1具有较好的质量。EDAX分析表明,In2Se3晶体由In和Se元素组成,摩尔比为2:9,而SEM表征表明,In2Se3晶体表面形貌颜色不均匀。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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