Magnetic Barkhausen Noise Measurements on Rocks

Tecnura Pub Date : 2022-07-01 DOI:10.14483/22487638.17148
Miriam Rocío Neyra Astudillo, María Isabel López-Pumarega, Silvana Evangelina-Geuna, Martín Gómez
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Abstract

Context: The magnetic properties of rocks may reflect the modal abundance, composition, and microstructure of the magnetic grains contained within them, usually in a very small proportion. Magnetic Barkhausen Noise (MBN) is a non-destructive technique applied to magnetic materials, and it is very sensitive to microstructure and residual stresses. In this work, measurements of MBN in samples of rocks extracted from nature and containing varying proportions of magnetite were studied and analyzed. Method: Measurements were taken by magnetically exciting the cylindrical samples, using a magnetic yoke and measuring the induced field inside the rock as a consequence of the excitation. For the detection, a sensor coil placed on the excited surface on one of the flat faces of each cylinder was used. The signals obtained from the MBN were digitized, and a digital 5-200 kHz Butterworth filter was applied, calculating the root mean square (RMS) values. Results: The linear fit of the MBN RMS values with the increasing percentage of ferromagnetic minerals showed an increasing trend with a moderate correlation. A correlation between coercive force and the MBN RMS values was observed only for samples with abundant magnetite (> 25 vol%). Conclusions: An increasing variation of the RMS values of the MBN signals was observed in relation with coercive force for abundant magnetite samples. This may be related to the geological processes involved in magnetite genesis. Method: The measurements were made exciting magnetically the samples (cylindrical shapes), using a magnetic yoke and measuring the induced field inside the rock as a result of the excitation. For the detection, a sensor coil placed on the excited surface on one of the flat faces of each cylinder was used. The signals obtained from MBN were digitized. A digital 5-200 kHz Butterworth filter was applied and the RMS (Root Mean Square) values were calculated. Results: The linear fit of the MBN RMS values with the increasing percentage of ferromagnetic minerals showed an increasing trend with moderate correlation. A correlation between coercive force and MBN RMS was observed only for samples with abundant magnetite (> 25 vol%). Conclusions: A variation of the RMS values of the MBN signals was observed in relation with coercive force for massive magnetite samples. This can be related to geological processes involved in magnetite genesis.   Keywords: Rocks, Magnetization, Barkhausen Magnetic Noise, Non-Destructive Test.  
岩石巴克豪森磁噪声测量
背景:岩石的磁性能可以反映其中所含磁性颗粒的丰度、组成和微观结构,通常比例很小。磁巴克豪森噪声(MBN)是一种应用于磁性材料的无损检测技术,它对微观结构和残余应力非常敏感。在这项工作中,研究和分析了从自然界中提取的含有不同比例磁铁矿的岩石样品的MBN测量。方法:利用磁轭对圆柱形样品进行磁激励,测量岩石内部由于激励而产生的感应场。为了进行检测,将传感器线圈放置在每个圆柱体的一个平面上的激励表面上。对从MBN获得的信号进行数字化处理,并应用5-200 kHz巴特沃斯数字滤波器,计算均方根(RMS)值。结果:MBN RMS值随铁磁性矿物含量的增加线性拟合呈增加趋势,相关性中等。仅在磁铁矿丰富的样品中(> 25 vol%),矫顽力与MBN RMS值之间存在相关性。结论:在磁铁矿丰富的样品中,MBN信号的均方根值随矫顽力的增大而增大。这可能与磁铁矿成因的地质作用有关。方法:利用磁轭对样品(圆柱形)进行磁激励,测量岩石内部因激励而产生的感应场。为了进行检测,将传感器线圈放置在每个圆柱体的一个平面上的激励表面上。对MBN接收到的信号进行数字化处理。应用数字5-200 kHz巴特沃斯滤波器并计算RMS(均方根)值。结果:MBN RMS值随铁磁性矿物含量的增加线性拟合呈增加趋势,相关性中等。仅在磁铁矿丰富的样品(> 25 vol%)中观察到矫顽力与MBN RMS之间的相关性。结论:块状磁铁矿样品中MBN信号的均方根值随矫顽力的变化而变化。这可能与磁铁矿成因的地质作用有关。关键词:岩石,磁化,巴克豪森磁噪声,无损检测
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