{"title":"Electron Probe Microanalysis In Geosciences: Analytical Procedures And Recent Advances","authors":"Shuiyuan Yang","doi":"10.46770/as.2021.912","DOIUrl":null,"url":null,"abstract":"Electron probe microanalysis (EPMA) is an in-situ and non-destructive analytical technique with high spatial resolution and an increasingly important analysis tool in materials science and geosciences. This study summarizes the principles and functions of EPMA, and the problems and difficulties, along with the recent advances in quantitative analysis of EPMA. A routine EPMA procedure includes preparing samples, setting analytical conditions, acquiring data, and evaluating results. Caution is required in all steps to obtain high-quality analytical results. The problems and difficulties commonly encountered in EPMA are discussed and the corresponding measures and solutions required to resolve them are proposed. Specific analytical methods are suggested to make accurate analysis of some specific minerals. We also summarized the challenges and solutions in light element analysis, trace element analysis, EPMA U-Th-Pb total dating, combined analysis with wavelengthand energy-dispersive X-ray spectroscopy, submicron spatial resolution analysis at low accelerating voltages, iron oxidation state analysis, and standard reference materials.","PeriodicalId":8642,"journal":{"name":"Atomic Spectroscopy","volume":null,"pages":null},"PeriodicalIF":3.4000,"publicationDate":"2022-01-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"12","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Atomic Spectroscopy","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.46770/as.2021.912","RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"SPECTROSCOPY","Score":null,"Total":0}
引用次数: 12
Abstract
Electron probe microanalysis (EPMA) is an in-situ and non-destructive analytical technique with high spatial resolution and an increasingly important analysis tool in materials science and geosciences. This study summarizes the principles and functions of EPMA, and the problems and difficulties, along with the recent advances in quantitative analysis of EPMA. A routine EPMA procedure includes preparing samples, setting analytical conditions, acquiring data, and evaluating results. Caution is required in all steps to obtain high-quality analytical results. The problems and difficulties commonly encountered in EPMA are discussed and the corresponding measures and solutions required to resolve them are proposed. Specific analytical methods are suggested to make accurate analysis of some specific minerals. We also summarized the challenges and solutions in light element analysis, trace element analysis, EPMA U-Th-Pb total dating, combined analysis with wavelengthand energy-dispersive X-ray spectroscopy, submicron spatial resolution analysis at low accelerating voltages, iron oxidation state analysis, and standard reference materials.
期刊介绍:
The ATOMIC SPECTROSCOPY is a peer-reviewed international journal started in 1962 by Dr. Walter Slavin and now is published by Atomic Spectroscopy Press Limited (ASPL). It is intended for the rapid publication of both original articles and review articles in the fields of AAS, AFS, ICP-OES, ICP-MS, GD-MS, TIMS, SIMS, AMS, LIBS, XRF and related techniques. Manuscripts dealing with (i) instrumentation & fundamentals, (ii) methodology development & applications, and (iii) standard reference materials (SRMs) development can be submitted for publication.