Effect of Universal Adhesives on Long-term Bond Strength to Zirconia.

IF 2.5 3区医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE

Journal of Adhesive Dentistry Pub Date : 2022-10-24 DOI:10.3290/j.jad.b3512333

Renata Vasconcelos Monteiro, Daniela Micheline Dos Santos, Bruna Chrispim, Jussara Karina Bernardon, Thiago Soares Porto, Grace Mendonça De Souza

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引用次数: 0

Abstract

Purpose: To evaluate the effect of universal adhesives on the long-term bond strength to yttria-stabilized tetragonal zirconia polycrystal (Y-TZP).

Materials and methods: Polyethylene tubes filled with composite cement containing 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) were adhesively luted to 60 fully sintered Y-TZP slabs (7 x 7 x 2 mm) with or without (control) previous application of a 10-MDP-based adhesive (All Bond Universal, Bisco) - ABU; Clearfil Universal Bond Quick, Kuraray Noritake - CUB; Scotchbond Universal Adhesive, 3M Oral Care - SUA) on the zirconia surface. The bonded specimens were stored in water for 24 h, 6 months, or 1 year and subjected to microshear bond strength testing. The data were analyzed by one-way ANOVA and Tukey's test (p < 0.05). The contact angle was measured after adhesive application to evaluate surface wettability. The adhesive-treated specimens were analyzed with x-ray photoelectron spectroscopy (XPS) and time-of-flight secondary ion mass spectrometry (ToF-SIMS) for chemical characterization.

Results: The application of a 10-MDP-based adhesive significantly improved bond strength of composite cement to zirconia when compared to the control group (no adhesive application) (p < 0.05). One-year water storage significantly decreased bond strength for ABU- and CUB-bonded specimens, but not for SUA-bonded specimens. The analysis by XPS and ToF-SIMS showed peaks of carbon, phosphorus, and silicon in all adhesive-treated specimens.

Conclusions: One-year water storage affected the bond strength of composite cement to zirconia when All Bond Universal or Clearfil Universal Bond Quick were used.

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通用粘合剂对氧化锆长期粘接强度的影响

目的：评估通用粘合剂对钇稳定四方氧化锆多晶体（Y-TZP）长期粘合强度的影响：将装有含 10-甲基丙烯酰氧癸基磷酸二氢酯（10-MDP）的复合粘合剂的聚乙烯管与 60 块完全烧结的 Y-TZP 板（7 x 7 x 2 毫米）粘接在一起，并在氧化锆表面涂抹或不涂抹（对照组）以 10-MDP 为基础的粘合剂（All Bond Universal，Bisco）- ABU；Clearfil Universal Bond Quick，Kuraray Noritake - CUB；Scotchbond Universal Adhesive，3M Oral Care - SUA）。粘结后的试样在水中分别存放 24 小时、6 个月或 1 年，然后进行微剪切粘结强度测试。数据分析采用单因素方差分析和 Tukey 检验（P < 0.05）。使用粘合剂后测量接触角以评估表面润湿性。用 X 射线光电子能谱（XPS）和飞行时间二次离子质谱（ToF-SIMS）分析粘合剂处理过的试样的化学特性：与对照组（未使用粘合剂）相比，使用基于 10-MDP 的粘合剂可显著提高复合水泥与氧化锆的粘结强度（p < 0.05）。ABU和CUB粘结试样一年的水贮存会明显降低粘结强度，而SUA粘结试样则不会。XPS 和 ToF-SIMS 分析显示，在所有粘合剂处理过的试样中都出现了碳、磷和硅的峰值：结论：使用 All Bond Universal 或 Clearfil Universal Bond Quick 时，一年的储水会影响复合水泥与氧化锆的粘接强度。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Journal of Adhesive Dentistry 医学-牙科与口腔外科

CiteScore

5.20

自引率

6.10%

发文量

审稿时长

6-12 weeks

期刊介绍： New materials and applications for adhesion are profoundly changing the way dentistry is delivered. Bonding techniques, which have long been restricted to the tooth hard tissues, enamel, and dentin, have obvious applications in operative and preventive dentistry, as well as in esthetic and pediatric dentistry, prosthodontics, and orthodontics. The current development of adhesive techniques for soft tissues and slow-releasing agents will expand applications to include periodontics and oral surgery. Scientifically sound, peer-reviewed articles explore the latest innovations in these emerging fields.