Modular and reconfigurable gas chromatography / differential mobility spectrometry (GC/DMS) package for detection of volatile organic compounds (VOCs).

Q3 Chemistry
Ilya M Anishchenko, Mitchell M McCartney, Alexander G Fung, Daniel J Peirano, Michael J Schirle, Nicholas J Kenyon, Cristina E Davis
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引用次数: 6

Abstract

Due to the versatility of present day microcontroller boards and open source development environments, new analytical chemistry devices can now be built outside of large industry and instead within smaller individual groups. While there are a wide range of commercial devices available for detecting and identifying volatile organic compounds (VOCs), most of these devices use their own proprietary software and complex custom electronics, making modifications or reconfiguration of the systems challenging. The development of microprocessors for general use, such as the Arduino prototyping platform, now enables custom chemical analysis instrumentation. We have created an example system using commercially available parts, centered around on differential mobility spectrometer (DMS) device. The Modular Reconfigurable Gas Chromatography - Differential Mobility Spectrometry package (MR-GC-DMS) has swappable components allowing it to be quickly reconfigured for specific application purposes as well as broad, generic use. The MR-GC-DMS has a custom user-friendly graphical user interface (GUI) and precisely tuned proportional-integral-derivative controller (PID) feedback control system managing individual temperature-sensitive components. Accurate temperature control programmed into the microcontroller greatly increases repeatability and system performance. Together, this open-source platform enables researchers to quickly combine DMS devices in customized configurations for new chemical sensing applications.

Abstract Image

Abstract Image

Abstract Image

模块化和可重构气相色谱/差分迁移率光谱(GC/DMS)包检测挥发性有机化合物(VOCs)。
由于当今微控制器板和开源开发环境的多功能性,新的分析化学设备现在可以在大型工业之外构建,而不是在较小的个人团体中构建。虽然有各种各样的商用设备可用于检测和识别挥发性有机化合物(VOCs),但这些设备大多使用自己的专有软件和复杂的定制电子设备,这使得系统的修改或重新配置具有挑战性。通用微处理器的开发,如Arduino原型平台,现在可以定制化学分析仪器。我们已经创建了一个例子系统,使用市购部件,以差分迁移率光谱仪(DMS)装置为中心。模块化可重构气相色谱-差分迁移率光谱包(MR-GC-DMS)具有可互换的组件,允许其快速重新配置特定的应用目的以及广泛的通用用途。MR-GC-DMS具有定制的用户友好图形用户界面(GUI)和精确调谐的比例-积分-导数控制器(PID)反馈控制系统,管理各个温度敏感组件。精确的温度控制写入微控制器,大大提高了可重复性和系统性能。总之,这个开源平台使研究人员能够快速组合DMS设备的定制配置,用于新的化学传感应用。
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来源期刊
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期刊介绍: The journal is devoted to all aspects of the mobility, reaction chemistry, and behavior of ions in a supporting gaseous atmosphere and in an electrical field. Articles span a broad range of research and arenas, e.g. laboratory studies of biomolecules at comparatively low pressure, instrumentation for field and process monitoring, and measurements of samples with relevance to industry, the environment, medicine, and security. The published papers cover theoretical and experimental findings from fundamental and applied studies including topics on chemistry, physics, geology, life sciences, and engineering associated with the measurement of ion mobility. In addition, papers and technical notes on novel instrument design, related new applications, and their validation are welcome.
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