Yan Ren, Xiang-ming Chen, Juan-juan Zhao, Chang-jun Lv
{"title":"[Study on Chemical Constituents and Content Determination of Feifukang Mistura].","authors":"Yan Ren, Xiang-ming Chen, Juan-juan Zhao, Chang-jun Lv","doi":"","DOIUrl":null,"url":null,"abstract":"<p><strong>Objective: </strong>To identify the main chemical constituents and to determine the content in Feifukang mistura.</p><p><strong>Methods: </strong>HPLC-MS technique was used to profile and identify the chemical constituents by comparing the retention time,MS data with the reference standard. The content determination of all the chemical constituents were carried on a HPLC system.</p><p><strong>Results: </strong>Five compounds were separated from Feifukang mistura,which were identified as neomangiferin,mangiferin,calycosin-7-O-glucoside,calycosin,and schizandrol A. The standard curves of them showed good linearity on the range of 2. 08 ~ 104. 0 μg/m L,2. 00 ~ 100. 0 μg/m L,2. 00 ~ 100. 0μg/m L,2. 09 ~ 104. 5 μg/m L,and 1. 98 ~ 99. 0 μg/m L,respectively. The average recoveries were all in the range of 91. 3 ~ 103. 8%.</p><p><strong>Conclusion: </strong>The methods of chemical constituents identification and content determination were established,which may offer better revealing the material basis and controlling quality of Feifukang mistura.</p>","PeriodicalId":15312,"journal":{"name":"中药材","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2016-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"中药材","FirstCategoryId":"3","ListUrlMain":"","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Objective: To identify the main chemical constituents and to determine the content in Feifukang mistura.
Methods: HPLC-MS technique was used to profile and identify the chemical constituents by comparing the retention time,MS data with the reference standard. The content determination of all the chemical constituents were carried on a HPLC system.
Results: Five compounds were separated from Feifukang mistura,which were identified as neomangiferin,mangiferin,calycosin-7-O-glucoside,calycosin,and schizandrol A. The standard curves of them showed good linearity on the range of 2. 08 ~ 104. 0 μg/m L,2. 00 ~ 100. 0 μg/m L,2. 00 ~ 100. 0μg/m L,2. 09 ~ 104. 5 μg/m L,and 1. 98 ~ 99. 0 μg/m L,respectively. The average recoveries were all in the range of 91. 3 ~ 103. 8%.
Conclusion: The methods of chemical constituents identification and content determination were established,which may offer better revealing the material basis and controlling quality of Feifukang mistura.
期刊介绍：
"Chinese Materia Medica" magazine was founded in 1978. It is a national-level academic journal of Chinese medicine science and technology approved by the State Science and Technology Commission and the Press and Publication Administration for public distribution at home and abroad. It is sponsored by the Chinese Materia Medica Information Center of the State Food and Drug Administration and is publicly distributed at home and abroad. It mainly reports on new technologies, new methods and new achievements in the production, scientific research and business management of Chinese medicine, and serves to promote the production and scientific and technological development of Chinese medicine, improve the output and quality of Chinese medicine, improve business management, and prosper the Chinese medicine industry.
求助内容：
应助结果提醒方式：
京公网安备 11010802042870号
