Structure and fluorometric HPLC determination of 1-desulfoyessotoxin, a new yessotoxin analog isolated from mussels from Norway.

M Daiguji, M Satake, H Ramstad, T Aune, H Naoki, T Yasumoto
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引用次数: 43

Abstract

A new analog of yessotoxin, 1-desulfoyessotoxin, was isolated from the digestive glands of mussels growing in the Sognefjord, Norway. Its structure was determined by NMR and negative ion CID MS/MS experiments. 1-Desulfoyessotoxin can be detected by the fluorometric HPLC method analogous with other yessotoxins.

挪威贻贝中一种新的类似物- 1-desulfoyessotoxin的结构和荧光高效液相色谱测定。
从生长在挪威Sognefjord的贻贝的消化腺中分离出一种新的yessosotoxin类似物- 1-desulfoyessotoxin。通过NMR和负离子CID MS/MS实验对其结构进行了表征。1 .用荧光高效液相色谱法可测定脱硫毒素的含量。
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